tert-butyl 2,2',2'',2'''-(4-bromo-1,2-phenylene)bis(azanetriyl)tetraacetate

Base Information

Chemical Name:tert-butyl 2,2',2'',2'''-(4-bromo-1,2-phenylene)bis(azanetriyl)tetraacetate
CAS No.:1610690-87-3
Molecular Formula:C₃₀H₄₇BrN₂O₈
Molecular Weight:643.616
Hs Code.:

Synonyms:tert-butyl 2,2',2'',2'''-(4-bromo-1,2-phenylene)bis(azanetriyl)tetraacetate

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Chemical Property of tert-butyl 2,2',2'',2'''-(4-bromo-1,2-phenylene)bis(azanetriyl)tetraacetate

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Technology Process of tert-butyl 2,2',2'',2'''-(4-bromo-1,2-phenylene)bis(azanetriyl)tetraacetate

There total 3 articles about tert-butyl 2,2',2'',2'''-(4-bromo-1,2-phenylene)bis(azanetriyl)tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1610690-86-2
C₃₀H₄₈N₂O₈

: 1610690-87-3
tert-butyl 2,2',2'',2'''-(4-bromo-1,2-phenylene)bis(azanetriyl)tetraacetate

Guidance literature:: With Oxone; potassium bromide; In methanol; at 20 ℃; for 4h;
DOI:10.1021/ja502406x

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1610690-87-3
tert-butyl 2,2',2'',2'''-(4-bromo-1,2-phenylene)bis(azanetriyl)tetraacetate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / acetonitrile / 84 h / 60 °C / Inert atmosphere

2: potassium bromide; Oxone / methanol / 4 h / 20 °C

With Oxone; N-ethyl-N,N-diisopropylamine; potassium bromide; In methanol; acetonitrile;
DOI:10.1021/ja502406x

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 1610690-87-3
tert-butyl 2,2',2'',2'''-(4-bromo-1,2-phenylene)bis(azanetriyl)tetraacetate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / acetonitrile / 84 h / 60 °C / Inert atmosphere

2: potassium bromide; Oxone / methanol / 4 h / 20 °C

With Oxone; N-ethyl-N,N-diisopropylamine; potassium bromide; In methanol; acetonitrile;
DOI:10.1021/ja502406x