N-benzyl-N-(1-cyclohexyl-4,4,4-trifluorobut-2-ynyl)hydroxylamine

Base Information

• Chemical Name: N-benzyl-N-(1-cyclohexyl-4,4,4-trifluorobut-2-ynyl)hydroxylamine
• CAS No.: 1170994-16-7
• Molecular Formula: C₁₇H₂₀F₃NO
• Molecular Weight: 311.347
• Mol file: 1170994-16-7.mol

Synonyms:N-benzyl-N-(1-cyclohexyl-4,4,4-trifluorobut-2-ynyl)hydroxylamine

Chemical Property of N-benzyl-N-(1-cyclohexyl-4,4,4-trifluorobut-2-ynyl)hydroxylamine

Chemical Property:

Purity/Quality:

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Technology Process of N-benzyl-N-(1-cyclohexyl-4,4,4-trifluorobut-2-ynyl)hydroxylamine

There total 1 articles about N-benzyl-N-(1-cyclohexyl-4,4,4-trifluorobut-2-ynyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-bromo-3,3,3-trifluoropropene (1514-82-5) + N-cyclohexylidenebenzylamine N-oxide (22687-06-5) → N-benzyl-N-(1-cyclohexyl-4,4,4-trifluorobut-2-ynyl)hydroxylamine (1170994-16-7)

Guidance literature:

2-bromo-3,3,3-trifluoropropene; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

N-cyclohexylidenebenzylamine N-oxide; In tetrahydrofuran; at -20 ℃; for 2h;

DOI:10.1055/s-0028-1087988

Reference yield: 59.0%

N-benzyl-N-(1-cyclohexyl-4,4,4-trifluorobut-2-ynyl)hydroxylamine (1170994-16-7) → N-benzyl-N-(1-cyclohexyl-4,4,4-trifluorobut-2-ynyl)amine (1170994-50-9)

Guidance literature:

With phosphorus trichloride; In benzene; at 20 ℃; for 7h;

DOI:10.1055/s-0028-1087988

upstream raw materials:

2-bromo-3,3,3-trifluoropropene

N-cyclohexylidenebenzylamine N-oxide

Downstream raw materials:

N-benzyl-N-(1-cyclohexyl-4,4,4-trifluorobut-2-ynyl)amine