(2Z)-5-[[(1E,2E)-2-[2,2-bis(ethoxycarbonyl)hydrazono]-1-methylpropylidene]amino]-3-(4-chlorophenyl)-2-(cyclohexylimino)-2,3-dihydro-1,3,4-thiadiazole

Base Information

• Chemical Name: (2Z)-5-[[(1E,2E)-2-[2,2-bis(ethoxycarbonyl)hydrazono]-1-methylpropylidene]amino]-3-(4-chlorophenyl)-2-(cyclohexylimino)-2,3-dihydro-1,3,4-thiadiazole
• CAS No.: 1435872-34-6
• Molecular Formula: C₂₄H₃₁ClN₆O₄S
• Molecular Weight: 535.067

Synonyms:(2Z)-5-[[(1E,2E)-2-[2,2-bis(ethoxycarbonyl)hydrazono]-1-methylpropylidene]amino]-3-(4-chlorophenyl)-2-(cyclohexylimino)-2,3-dihydro-1,3,4-thiadiazole

Chemical Property of (2Z)-5-[[(1E,2E)-2-[2,2-bis(ethoxycarbonyl)hydrazono]-1-methylpropylidene]amino]-3-(4-chlorophenyl)-2-(cyclohexylimino)-2,3-dihydro-1,3,4-thiadiazole

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Technology Process of (2Z)-5-[[(1E,2E)-2-[2,2-bis(ethoxycarbonyl)hydrazono]-1-methylpropylidene]amino]-3-(4-chlorophenyl)-2-(cyclohexylimino)-2,3-dihydro-1,3,4-thiadiazole

There total 1 articles about (2Z)-5-[[(1E,2E)-2-[2,2-bis(ethoxycarbonyl)hydrazono]-1-methylpropylidene]amino]-3-(4-chlorophenyl)-2-(cyclohexylimino)-2,3-dihydro-1,3,4-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

Cyclohexyl isocyanide (931-53-3) + 1-[(4-chlorophenyl)amino]-1,3-dihydro-4,5-dimethyl-2H-imidazole-2-thione (1022903-95-2) + diethylazodicarboxylate (1972-28-7,218603-74-8) → (2Z)-5-[[(1E,2E)-2-[2,2-bis(ethoxycarbonyl)hydrazono]-1-methylpropylidene]amino]-3-(4-chlorophenyl)-2-(cyclohexylimino)-2,3-dihydro-1,3,4-thiadiazole (1435872-34-6)

Guidance literature:

In toluene; for 2h; Reflux;

DOI:10.1016/j.tet.2013.03.096

Reference yield: 77.0%

(2Z)-5-[[(1E,2E)-2-[2,2-bis(ethoxycarbonyl)hydrazono]-1-methylpropylidene]amino]-3-(4-chlorophenyl)-2-(cyclohexylimino)-2,3-dihydro-1,3,4-thiadiazole (1435872-34-6) → (2Z)-3-(4-chlorophenyl)-2-(cyclohexylimino)-5-[[(1E,2E)-2-[2-(ethoxycarbonyl)hydrazono]-1-methylpropylidene]amino]-2,3-dihydro-1,3,4-thiadiazole (1435872-52-8)

Guidance literature:

With sodium cyanoborohydride; In methanol; at 20 ℃; for 2h;

DOI:10.1016/j.tet.2013.03.096

upstream raw materials:

Cyclohexyl isocyanide

1-[(4-chlorophenyl)amino]-1,3-dihydro-4,5-dimethyl-2H-imidazole-2-thione

diethylazodicarboxylate

Downstream raw materials:

(2Z)-3-(4-chlorophenyl)-2-(cyclohexylimino)-5-[[(1E,2E)-2-[2-(ethoxycarbonyl)hydrazono]-1-methylpropylidene]amino]-2,3-dihydro-1,3,4-thiadiazole

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