((H₅C₆NC(Me))2CH)Al(H)(neopentyl)

Base Information

Chemical Name:((H₅C₆NC(Me))2CH)Al(H)(neopentyl)
CAS No.:1154406-21-9
Molecular Formula:C₂₂H₂₉AlN₂
Molecular Weight:348.467
Hs Code.:

((H<sub>5</sub>C<sub>6</sub>NC(Me))2CH)Al(H)(neopentyl)

Synonyms:((H₅C₆NC(Me))2CH)Al(H)(neopentyl)

Suppliers and Price of ((H₅C₆NC(Me))2CH)Al(H)(neopentyl)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ((H₅C₆NC(Me))2CH)Al(H)(neopentyl)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ((H₅C₆NC(Me))2CH)Al(H)(neopentyl)

There total 2 articles about ((H₅C₆NC(Me))2CH)Al(H)(neopentyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 281654-52-2
(Ph₂-nacnac)AlH₂

: 7412-67-1
neopentyl lithium

: 1154406-21-9
((H₅C₆NC(Me))2CH)Al(H)(neopentyl)

Guidance literature:: In Cyclopentane; byproducts: LiH; (Ar); treatment of cooled soln. (-40°C) of AlH2((NPhCMe)2CH) in cyclopentane with equimolar quantities neopentyllithium; slow warming to room temp.; stirring overnight; removal of solvent in vac., treatment with n-pentane; filtration, cooling to -30°C; crystn., elem. anal.;
DOI:10.1016/j.jorganchem.2008.09.036

Reference yield:

: 2-N-phenylamino-4-N-phenylimino-2-pentene

: 1154406-21-9
((H₅C₆NC(Me))2CH)Al(H)(neopentyl)

Guidance literature:: Multi-step reaction with 2 steps

1: not given

2: Cyclopentane

In Cyclopentane;
DOI:10.1016/j.jorganchem.2008.09.036

Reference yield: 79.0%

: 75-91-2
tert.-butylhydroperoxide

: 1154406-21-9
((H₅C₆NC(Me))2CH)Al(H)(neopentyl)

: 1154406-25-3
((H₅C₆NC(Me))2CHAl(neopentyl))2O

Guidance literature:: In nonane; hexane; byproducts: hydrogen, HOC(CH3)3; (Ar); addn. dropwise of soln. of Me3COOH in nonane to cooled soln. (-78°C) of AlH(CH2CMe3)((NPhCMe)2CH) in n-hexane; slow warming to -10°C and concn.; crystn. at -15°C for 2 d; elem. anal.;
DOI:10.1016/j.jorganchem.2008.09.036