O,O'-dibutyl {[2-(2-chloro-4-fluorophenoxy)acetamido](phenyl)methyl}phosphonate

Base Information

Chemical Name:O,O'-dibutyl {[2-(2-chloro-4-fluorophenoxy)acetamido](phenyl)methyl}phosphonate
CAS No.:1357284-98-0
Molecular Formula:C₂₃H₃₀ClFNO₅P
Molecular Weight:485.92
Hs Code.:

Synonyms:O,O'-dibutyl {[2-(2-chloro-4-fluorophenoxy)acetamido](phenyl)methyl}phosphonate

Suppliers and Price of O,O'-dibutyl {[2-(2-chloro-4-fluorophenoxy)acetamido](phenyl)methyl}phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O,O'-dibutyl {[2-(2-chloro-4-fluorophenoxy)acetamido](phenyl)methyl}phosphonate

Chemical Property:

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Technology Process of O,O'-dibutyl {[2-(2-chloro-4-fluorophenoxy)acetamido](phenyl)methyl}phosphonate

There total 4 articles about O,O'-dibutyl {[2-(2-chloro-4-fluorophenoxy)acetamido](phenyl)methyl}phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: (α-amino-benzyl)-phosphonic acid dibutyl ester

: 826990-46-9
2-(2-chloro-4-fluorophenoxy)acetyl chloride

: 1357284-98-0
O,O'-dibutyl {[2-(2-chloro-4-fluorophenoxy)acetamido](phenyl)methyl}phosphonate

Guidance literature:: With pyridine; In dichloromethane; at 2 - 20 ℃; for 3h;
DOI:10.1016/j.ejmech.2011.12.014

Reference yield:

: 100-52-7
benzaldehyde

: 1357284-98-0
O,O'-dibutyl {[2-(2-chloro-4-fluorophenoxy)acetamido](phenyl)methyl}phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonium hydroxide / water / 5 h / Reflux

2.1: 70 °C

3.1: toluene-4-sulfonic acid / tetrahydrofuran / 2 h / 0 °C

3.2: 0.5 h / 20 °C

4.1: pyridine / dichloromethane / 3 h / 2 - 20 °C

With pyridine; ammonium hydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.ejmech.2011.12.014

Reference yield:

: 1038997-69-1
C₂₂H₃₀NO₃P

: 1357284-98-0
O,O'-dibutyl {[2-(2-chloro-4-fluorophenoxy)acetamido](phenyl)methyl}phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / tetrahydrofuran / 2 h / 0 °C

1.2: 0.5 h / 20 °C

2.1: pyridine / dichloromethane / 3 h / 2 - 20 °C

With pyridine; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ejmech.2011.12.014