methyl 2-(2-benzoyl-2-methylhydrazinyl)-4-(tert-butyldimethylsilyloxy)-2-methyl-butanoate

Base Information

Chemical Name:methyl 2-(2-benzoyl-2-methylhydrazinyl)-4-(tert-butyldimethylsilyloxy)-2-methyl-butanoate
CAS No.:1029435-34-4
Molecular Formula:C₂₀H₃₄N₂O₄Si
Molecular Weight:394.586
Hs Code.:

Synonyms:methyl 2-(2-benzoyl-2-methylhydrazinyl)-4-(tert-butyldimethylsilyloxy)-2-methyl-butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-(2-benzoyl-2-methylhydrazinyl)-4-(tert-butyldimethylsilyloxy)-2-methyl-butanoate

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Technology Process of methyl 2-(2-benzoyl-2-methylhydrazinyl)-4-(tert-butyldimethylsilyloxy)-2-methyl-butanoate

There total 1 articles about methyl 2-(2-benzoyl-2-methylhydrazinyl)-4-(tert-butyldimethylsilyloxy)-2-methyl-butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1029435-28-6
methyl (E)-2-(2-benzoyl-2-methylhydrazono)propanoate

: 101166-65-8
2-tert-butyldimethylsilyloxyethyl iodide

: 1029435-34-4
methyl 2-(2-benzoyl-2-methylhydrazinyl)-4-(tert-butyldimethylsilyloxy)-2-methyl-butanoate

Guidance literature:: methyl (E)-2-(2-benzoyl-2-methylhydrazono)propanoate; With indium(III) chloride; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

2-tert-butyldimethylsilyloxyethyl iodide; With dimanganese decacarbonyl; dichloromethane; at 35 ℃; Inert atmosphere; UV-irradiation;
DOI:10.1021/ol800733b

Reference yield: 67.0%

: 1029435-34-4
methyl 2-(2-benzoyl-2-methylhydrazinyl)-4-(tert-butyldimethylsilyloxy)-2-methyl-butanoate

: 88070-48-8
N-methylbenzamide

: C₁₂H₂₇NO₃Si

Guidance literature:: methyl 2-(2-benzoyl-2-methylhydrazinyl)-4-(tert-butyldimethylsilyloxy)-2-methyl-butanoate; With samarium diiodide; In tetrahydrofuran; methanol; at -78 - 20 ℃; for 2h; Inert atmosphere;

With acetic acid; In tetrahydrofuran; methanol; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol800733b