N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-methylsulfanylacetamide

Base Information

Chemical Name:N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-methylsulfanylacetamide
CAS No.:1425942-37-5
Molecular Formula:C₂₁H₁₇Cl₃F₃NO₂S
Molecular Weight:510.792
Hs Code.:

Synonyms:N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-methylsulfanylacetamide

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Chemical Property of N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-methylsulfanylacetamide

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Technology Process of N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-methylsulfanylacetamide

There total 5 articles about N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-methylsulfanylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2444-37-3
methylsulfanyl-acetic acid

: 1425942-92-2
[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methanamine

: 1425942-37-5
N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-methylsulfanylacetamide

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 1425942-96-6
2-[[2-chloro-4-[(E)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-hydroxy-but-1-enyl]phenyl]methyl]isoindoline-1,3-dione

: 1425942-37-5
N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-methylsulfanylacetamide

Guidance literature:: Multi-step reaction with 4 steps

1: dicarbonylacetylacetonato rhodium (I); tris(2,4-di-tert-butylphenyl)phosphite; hydrogen / tetrahydrofuran / 36 h / 100 °C / 37503.8 Torr / Inert atmosphere

2: toluene-4-sulfonic acid / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 130 °C / Inert atmosphere

3: hydrazine hydrate / ethanol / 0.33 h / 80 °C

4: triethylamine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C

With 1-hydroxy-7-aza-benzotriazole; dicarbonylacetylacetonato rhodium (I); tris(2,4-di-tert-butylphenyl)phosphite; hydrogen; toluene-4-sulfonic acid; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; dichloromethane;

Reference yield:

: 1425942-97-7
2-[[2-chloro-4-[5-(3,5-dichlorophenyl)-2-hydroxy-5-(trifluoromethyl)tetrahydrofuran-3-yl]phenyl]methyl]isoindoline-1,3-dione

: 1425942-37-5
N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-methylsulfanylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 130 °C / Inert atmosphere

2: hydrazine hydrate / ethanol / 0.33 h / 80 °C

3: triethylamine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C

With 1-hydroxy-7-aza-benzotriazole; toluene-4-sulfonic acid; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 5,5-dimethyl-1,3-cyclohexadiene; ethanol; dichloromethane;