4-(p-tolyldiazenyl)phenyl acrylate

Base Information

• Chemical Name: 4-(p-tolyldiazenyl)phenyl acrylate
• CAS No.: 3774-14-9
• Molecular Formula: C₁₆H₁₄N₂O₂
• Molecular Weight: 266.299
• Mol file: 3774-14-9.mol

Synonyms:4-(p-tolyldiazenyl)phenyl acrylate

Chemical Property of 4-(p-tolyldiazenyl)phenyl acrylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(p-tolyldiazenyl)phenyl acrylate

There total 3 articles about 4-(p-tolyldiazenyl)phenyl acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

acryloyl chloride (814-68-6,25189-84-8) + 4-((4-methylphenyl)azo)phenol (2497-33-8) → 4-(p-tolyldiazenyl)phenyl acrylate (3774-14-9)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1002/chem.201902273

Reference yield:

p-toluidine (106-49-0,12221-03-3) → 4-(p-tolyldiazenyl)phenyl acrylate (3774-14-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / acetone; water / 0.5 h / Cooling with ice

1.2: 2 h

2.1: triethylamine / dichloromethane / 20 °C

With hydrogenchloride; triethylamine; sodium nitrite; In dichloromethane; water; acetone;

DOI:10.1002/chem.201902273

Reference yield:

phenol (108-95-2,27073-41-2) → 4-(p-tolyldiazenyl)phenyl acrylate (3774-14-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / acetone; water / 0.5 h / Cooling with ice

1.2: 2 h

2.1: triethylamine / dichloromethane / 20 °C

With hydrogenchloride; triethylamine; sodium nitrite; In dichloromethane; water; acetone;

DOI:10.1002/chem.201902273

upstream raw materials:

acryloyl chloride

4-((4-methylphenyl)azo)phenol

p-toluidine

phenol