(-)-[bis-(1R,2S,5R)-(-)-menthyl] 1,3-acetonedicarboxylate

Base Information

Chemical Name:(-)-[bis-(1R,2S,5R)-(-)-menthyl] 1,3-acetonedicarboxylate
CAS No.:251565-32-9
Molecular Formula:C₂₅H₄₂O₅
Molecular Weight:422.605
Hs Code.:

Synonyms:(-)-[bis-(1R,2S,5R)-(-)-menthyl] 1,3-acetonedicarboxylate

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Chemical Property of (-)-[bis-(1R,2S,5R)-(-)-menthyl] 1,3-acetonedicarboxylate

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Technology Process of (-)-[bis-(1R,2S,5R)-(-)-menthyl] 1,3-acetonedicarboxylate

There total 2 articles about (-)-[bis-(1R,2S,5R)-(-)-menthyl] 1,3-acetonedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1830-54-2
3-oxopentanedioic acid dimethyl ester

: 2216-51-5
(-)-menthol

: 251565-32-9
(-)-[bis-(1R,2S,5R)-(-)-menthyl] 1,3-acetonedicarboxylate

Guidance literature:: With dmap; In toluene; for 6h; Heating;
DOI:10.1016/j.tetasy.2006.11.004

Reference yield: 92.0%

: 1830-54-2
3-oxopentanedioic acid dimethyl ester

: 464-45-9
endo-borneol

: 251565-32-9
(-)-[bis-(1R,2S,5R)-(-)-menthyl] 1,3-acetonedicarboxylate

Guidance literature:: With dmap; In cyclohexane; for 72h; Heating;
DOI:10.1002/(SICI)1099-0690(200004)2000:8<1633::AID-EJOC1633>3.0.CO;2-W

Reference yield: 90.0%

: 251565-32-9
(-)-[bis-(1R,2S,5R)-(-)-menthyl] 1,3-acetonedicarboxylate

: 144660-39-9
(R)-(-)-[bis-(1R,2S,5R)-(-)-menthyl] 2,3-pentadienedioate

Guidance literature:: (-)-[bis-(1R,2S,5R)-(-)-menthyl] 1,3-acetonedicarboxylate; With 1,3-dimethylimidazolin-3-ium hexafluorophosphate; triethylamine; In dichloromethane; for 1.5h;

With triethylamine; In pentane; at -20 ℃;
DOI:10.1016/j.tetasy.2006.11.004