3-(4-chlorophenyl)-glutaric acid monoethyl ester

Base Information

Chemical Name:3-(4-chlorophenyl)-glutaric acid monoethyl ester
CAS No.:860011-99-0
Molecular Formula:C₁₃H₁₅ClO₄
Molecular Weight:270.713
Hs Code.:

Synonyms:3-(4-chlorophenyl)-glutaric acid monoethyl ester

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Chemical Property of 3-(4-chlorophenyl)-glutaric acid monoethyl ester

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Technology Process of 3-(4-chlorophenyl)-glutaric acid monoethyl ester

There total 4 articles about 3-(4-chlorophenyl)-glutaric acid monoethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 64-17-5
ethanol

: 53911-68-5
3-(4-chlorophenyl)glutaric anhydride

: 860011-99-0
3-(4-chlorophenyl)-glutaric acid monoethyl ester

Guidance literature:: With pyridine; for 3h; Heating;
DOI:10.1016/j.tet.2005.04.032

Reference yield: 70.0%

: 64-17-5
ethanol

: 35271-74-0
3-(4-chlorophenyl)pentane-1,5-dioic acid

: 860011-99-0
3-(4-chlorophenyl)-glutaric acid monoethyl ester

Guidance literature:: 3-(4-chlorophenyl)pentane-1,5-dioic acid; With acetic anhydride; for 17h; Heating / reflux;

ethanol; With triethylamine; at 20 ℃; for 17h;

Reference yield:

: 35271-74-0
3-(4-chlorophenyl)pentane-1,5-dioic acid

: 860011-99-0
3-(4-chlorophenyl)-glutaric acid monoethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Ac₂O / Heating

2: Heating

With acetic anhydride;
DOI:10.1016/j.bmcl.2005.11.017