Pyrimidine, 1,4,5,6-tetrahydro-1-(2,4,6-trimethylphenyl)- (9CI)

Base Information

Chemical Name:Pyrimidine, 1,4,5,6-tetrahydro-1-(2,4,6-trimethylphenyl)- (9CI)
CAS No.:821779-94-6
Molecular Formula:C13H18 N2
Molecular Weight:202.299
Hs Code.:
Mol file:821779-94-6.mol

Synonyms:Pyrimidine, 1,4,5,6-tetrahydro-1-(2,4,6-trimethylphenyl)- (9CI)

Suppliers and Price of Pyrimidine, 1,4,5,6-tetrahydro-1-(2,4,6-trimethylphenyl)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Pyrimidine, 1,4,5,6-tetrahydro-1-(2,4,6-trimethylphenyl)- (9CI)

Chemical Property:

Melting Point:80 - 80.5 °C
PSA：15.60000
LogP:2.35080

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Pyrimidine, 1,4,5,6-tetrahydro-1-(2,4,6-trimethylphenyl)- (9CI)

There total 4 articles about Pyrimidine, 1,4,5,6-tetrahydro-1-(2,4,6-trimethylphenyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 149-73-5
trimethyl orthoformate

: 683811-55-4
N-(2,4,6-trimethylphenyl)-1,3-propanediamine

: 821779-94-6
1-(2,4,6-trimethylphenyl)-1,4,5,6-tetrahydropyrimidine

Guidance literature:: With hydrogen iodide; Heating;
DOI:10.1021/jo060594+

Reference yield:

: 909030-55-3
2-azido-N-mesitylpropionamide

: 821779-94-6
1-(2,4,6-trimethylphenyl)-1,4,5,6-tetrahydropyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / LiAlH₄ / tetrahydrofuran / Heating

2: 65 percent / HI / Heating

With lithium aluminium tetrahydride; hydrogen iodide; In tetrahydrofuran;
DOI:10.1021/jo060594+

Reference yield:

: 100141-43-3
N-(3'-chloropropionyl)mesitylamine

: 821779-94-6
1-(2,4,6-trimethylphenyl)-1,4,5,6-tetrahydropyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / NaN₃ / dimethylformamide / 80 °C

2: 67 percent / LiAlH₄ / tetrahydrofuran / Heating

3: 65 percent / HI / Heating

With lithium aluminium tetrahydride; sodium azide; hydrogen iodide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo060594+