2-(2-azidobenzenesulfonyl)-3,6-dihydro-4,5-dimethyl-1,2-thiazine 1-oxide

Base Information

Chemical Name:2-(2-azidobenzenesulfonyl)-3,6-dihydro-4,5-dimethyl-1,2-thiazine 1-oxide
CAS No.:791814-87-4
Molecular Formula:C₁₂H₁₄N₄O₃S₂
Molecular Weight:326.4
Hs Code.:

Synonyms:2-(2-azidobenzenesulfonyl)-3,6-dihydro-4,5-dimethyl-1,2-thiazine 1-oxide

Suppliers and Price of 2-(2-azidobenzenesulfonyl)-3,6-dihydro-4,5-dimethyl-1,2-thiazine 1-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-(2-azidobenzenesulfonyl)-3,6-dihydro-4,5-dimethyl-1,2-thiazine 1-oxide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-(2-azidobenzenesulfonyl)-3,6-dihydro-4,5-dimethyl-1,2-thiazine 1-oxide

There total 3 articles about 2-(2-azidobenzenesulfonyl)-3,6-dihydro-4,5-dimethyl-1,2-thiazine 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: C₆H₄N₄O₃S₂

: 791814-87-4
2-(2-azidobenzenesulfonyl)-3,6-dihydro-4,5-dimethyl-1,2-thiazine 1-oxide

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2004.08.136

Reference yield:

: 66081-21-8
2-azidobenzenesulphonamide

: 791814-87-4
2-(2-azidobenzenesulfonyl)-3,6-dihydro-4,5-dimethyl-1,2-thiazine 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; thionyl chloride / tetrahydrofuran / 3 h / 0 °C

2: tetrahydrofuran / 0 - 20 °C

With pyridine; thionyl chloride; In tetrahydrofuran; 2: hetero Diels-Alder reaction;
DOI:10.1016/j.tetlet.2004.08.136

Reference yield:

: 3306-62-5
2-AMINOBENZENESULFONAMIDE

: 791814-87-4
2-(2-azidobenzenesulfonyl)-3,6-dihydro-4,5-dimethyl-1,2-thiazine 1-oxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaNO₂; aq. HCl

1.2: NaN₃

2.1: pyridine; thionyl chloride / tetrahydrofuran / 3 h / 0 °C

3.1: tetrahydrofuran / 0 - 20 °C

With pyridine; hydrogenchloride; thionyl chloride; sodium nitrite; In tetrahydrofuran; 3.1: hetero Diels-Alder reaction;
DOI:10.1016/j.tetlet.2004.08.136