methyl 2-methyl-4-{[(4-methylphenyl)sulfonyl]oxy}-3-thiophenecarboxylate

Base Information

Chemical Name:methyl 2-methyl-4-{[(4-methylphenyl)sulfonyl]oxy}-3-thiophenecarboxylate
CAS No.:227312-08-5
Molecular Formula:C₁₄H₁₄O₅S₂
Molecular Weight:326.394
Hs Code.:
Mol file:227312-08-5.mol

Synonyms:2-methyl-4-((4-methylphenyl)sulfonyl)oxy-3-thiophenecarboxylic acid methyl ester

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Chemical Property of methyl 2-methyl-4-{[(4-methylphenyl)sulfonyl]oxy}-3-thiophenecarboxylate

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Technology Process of methyl 2-methyl-4-{[(4-methylphenyl)sulfonyl]oxy}-3-thiophenecarboxylate

There total 3 articles about methyl 2-methyl-4-{[(4-methylphenyl)sulfonyl]oxy}-3-thiophenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 227312-03-0
2,5-dihydro-2-methyl-4-((4-methylphenyl)sulfonyl)oxy-3-thiophenecarboxylic acid methyl ester

: 227312-08-5
2-methyl-4-((4-methylphenyl)sulfonyl)oxy-3-thiophenecarboxylic acid methyl ester

Guidance literature:: With sulfuryl dichloride; In dichloromethane; Ambient temperature;
DOI:10.1007/PL00010236

Reference yield:

: 65369-27-9
2-Methyl-4-oxo-tetrahydrothiophen-3-carbonsaeuremethylester

: 227312-08-5
2-methyl-4-((4-methylphenyl)sulfonyl)oxy-3-thiophenecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide / Ambient temperature

2: 71 percent / SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

With sulfuryl dichloride; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/PL00010236

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 227312-08-5
2-methyl-4-((4-methylphenyl)sulfonyl)oxy-3-thiophenecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide / Ambient temperature

2: 71 percent / SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

With sulfuryl dichloride; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/PL00010236