((2R,3S)-3-Benzyloxy-4-methylene-tetrahydro-thiophen-2-ylmethoxy)-tert-butyl-diphenyl-silane

Base Information

Chemical Name:((2R,3S)-3-Benzyloxy-4-methylene-tetrahydro-thiophen-2-ylmethoxy)-tert-butyl-diphenyl-silane
CAS No.:174833-56-8
Molecular Formula:C₂₉H₃₄O₂SSi
Molecular Weight:474.739
Hs Code.:

Synonyms:((2R,3S)-3-Benzyloxy-4-methylene-tetrahydro-thiophen-2-ylmethoxy)-tert-butyl-diphenyl-silane

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Chemical Property of ((2R,3S)-3-Benzyloxy-4-methylene-tetrahydro-thiophen-2-ylmethoxy)-tert-butyl-diphenyl-silane

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Technology Process of ((2R,3S)-3-Benzyloxy-4-methylene-tetrahydro-thiophen-2-ylmethoxy)-tert-butyl-diphenyl-silane

There total 5 articles about ((2R,3S)-3-Benzyloxy-4-methylene-tetrahydro-thiophen-2-ylmethoxy)-tert-butyl-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 174833-56-8
((2R,3S)-3-Benzyloxy-4-methylene-tetrahydro-thiophen-2-ylmethoxy)-tert-butyl-diphenyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / imidazole / dimethylformamide / Ambient temperature

2: acetic anhydride, DMSO / Ambient temperature

3: 1.) NaH, tert-amyl alcohol / 1.) THF, room temperature, 2 h, 2.) THF, room temperature, overnight

With 1H-imidazole; tert-Amyl alcohol; acetic anhydride; sodium hydride; dimethyl sulfoxide; In N,N-dimethyl-formamide;
DOI:10.1021/jo9700540

Reference yield:

: 160882-25-7
3-O-benzyl-1-deoxy-4-thio-D-arabino-furanose

: 174833-56-8
((2R,3S)-3-Benzyloxy-4-methylene-tetrahydro-thiophen-2-ylmethoxy)-tert-butyl-diphenyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / imidazole / dimethylformamide / Ambient temperature

2: acetic anhydride, DMSO / Ambient temperature

3: 1.) NaH, tert-amyl alcohol / 1.) THF, room temperature, 2 h, 2.) THF, room temperature, overnight

With 1H-imidazole; tert-Amyl alcohol; acetic anhydride; sodium hydride; dimethyl sulfoxide; In N,N-dimethyl-formamide;
DOI:10.1021/jo9700540

Reference yield:

: 174833-54-6
(3S,4S,5R)-4-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-thiophen-3-ol

: 174833-56-8
((2R,3S)-3-Benzyloxy-4-methylene-tetrahydro-thiophen-2-ylmethoxy)-tert-butyl-diphenyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: acetic anhydride, DMSO / Ambient temperature

2: 1.) NaH, tert-amyl alcohol / 1.) THF, room temperature, 2 h, 2.) THF, room temperature, overnight

With tert-Amyl alcohol; acetic anhydride; sodium hydride; dimethyl sulfoxide;
DOI:10.1021/jo9700540