phenyl 4-methoxybutyl sulfide

Base Information

• Chemical Name: phenyl 4-methoxybutyl sulfide
• CAS No.: 177416-33-0
• Molecular Formula: C₁₁H₁₆OS
• Molecular Weight: 196.313
• Mol file: 177416-33-0.mol

Synonyms:phenyl 4-methoxybutyl sulfide

Chemical Property of phenyl 4-methoxybutyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of phenyl 4-methoxybutyl sulfide

There total 2 articles about phenyl 4-methoxybutyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium thiophenolate (930-69-8) → phenyl 4-methoxybutyl sulfide (177416-33-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / methanol / 2 h / Heating

2: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, RT, 12 h

With sodium hydride; In methanol;

DOI:10.1016/0040-4020(96)00229-3

Reference yield:

4-(phenylthio)butan-1-ol (5851-37-6) + methyl iodide (74-88-4) → phenyl 4-methoxybutyl sulfide (177416-33-0)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) THF, RT, 1 h, 2.) THF, RT, 12 h;

DOI:10.1016/0040-4020(96)00229-3

Reference yield: 100.0%

phenyl 4-methoxybutyl sulfide (177416-33-0) → phenyl 4-methoxybutyl sulfone

Guidance literature:

With dihydrogen peroxide; acetic acid;

DOI:10.1021/ja001320l

upstream raw materials:

4-(phenylthio)butan-1-ol

methyl iodide

sodium thiophenolate

Downstream raw materials:

4-iodobutyl phenyl iodide