2-(bis(3,5-di-tert-butyl-2-hydroxybenzyl)amino) acetic acid

Base Information

• Chemical Name: 2-(bis(3,5-di-tert-butyl-2-hydroxybenzyl)amino) acetic acid
• CAS No.: 942592-70-3
• Molecular Formula: C₃₂H₄₉NO₄
• Molecular Weight: 511.745
• Mol file: 942592-70-3.mol

Synonyms:2-(bis(3,5-di-tert-butyl-2-hydroxybenzyl)amino) acetic acid

Chemical Property of 2-(bis(3,5-di-tert-butyl-2-hydroxybenzyl)amino) acetic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(bis(3,5-di-tert-butyl-2-hydroxybenzyl)amino) acetic acid

There total 2 articles about 2-(bis(3,5-di-tert-butyl-2-hydroxybenzyl)amino) acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2,4-di-tert-Butylphenol (96-76-4) + glycine (56-40-6,18875-39-3,25718-94-9) → 2-(bis(3,5-di-tert-butyl-2-hydroxybenzyl)amino) acetic acid (942592-70-3)

Guidance literature:

In water; for 48h; Reflux;

DOI:10.1016/j.poly.2011.01.036

Reference yield: 73.0%

2,4-di-tert-Butylphenol (96-76-4) + glycine (56-40-6,18875-39-3,25718-94-9) → 2-(bis(3,5-di-tert-butyl-2-hydroxybenzyl)amino) acetic acid (942592-70-3)

Guidance literature:

With sodium acetate; acetic acid; In water; for 6h;

DOI:10.1021/acs.inorgchem.1c00001

Reference yield:

2-(bis(3,5-di-tert-butyl-2-hydroxybenzyl)amino) acetic acid (942592-70-3) + dibutylmagnesium (1191-47-5) + triethylamine (121-44-8) + benzyl alcohol (100-51-6,185532-71-2) → [Mg4(2-(bis(3,5-di-tert-butyl-2-hydroxybenzyl)amino) acetate)3(BnOH)3]HNEt3*2H2O

Guidance literature:

2-(bis(3,5-di-tert-butyl-2-hydroxybenzyl)amino) acetic acid; triethylamine; In toluene; at 20 ℃; for 3h; Inert atmosphere;

dibutylmagnesium; benzyl alcohol; In hexane; toluene; for 12h; Inert atmosphere;

DOI:10.1039/c4dt03848g

upstream raw materials:

formaldehyd

2,4-di-tert-Butylphenol

glycine