(2-(Et₂NCH₂)-6-MeC₆H₃)AlH₂

Base Information

Chemical Name:(2-(Et₂NCH₂)-6-MeC₆H₃)AlH₂
CAS No.:289890-42-2
Molecular Formula:C₁₂H₂₀AlN
Molecular Weight:205.279
Hs Code.:

(2-(Et<sub>2</sub>NCH<sub>2</sub>)-6-MeC<sub>6</sub>H<sub>3</sub>)AlH<sub>2</sub>

Synonyms:(2-(Et₂NCH₂)-6-MeC₆H₃)AlH₂

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Chemical Property of (2-(Et₂NCH₂)-6-MeC₆H₃)AlH₂

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Technology Process of (2-(Et₂NCH₂)-6-MeC₆H₃)AlH₂

There total 1 articles about (2-(Et₂NCH₂)-6-MeC₆H₃)AlH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 16853-85-3
lithium aluminium tetrahydride

: 7446-70-0
aluminium trichloride

: 289890-47-7
2-(Et₂NCH₂)-6-MeC₆H₃Br

: 289890-42-2
(2-(Et₂NCH₂)-6-MeC₆H₃)AlH₂

Guidance literature:: With BuLi; In diethyl ether; hexane; under N2 soln. (2-(Et2NCH2)-6-C6H3)Li (from 2-(Et2NCH2-6-C6H3Br and BuLi in hexane) in Et2O was added to soln. AlCl3 in Et2O at -78°C, stirred overnight at room temp., filtered, added to suspn. LiAlH4 in Et2O, stirred 15 h at room temp.; volatiles were removed in vacuo, residue was extd. with n-hexane and concd.; elem. anal.;
DOI:10.1021/ic000255d