triethyl iodoorthoacetate

Base Information

• Chemical Name: triethyl iodoorthoacetate
• CAS No.: 183115-34-6
• Molecular Formula: C₈H₁₇IO₃
• Molecular Weight: 288.126

Synonyms:triethyl iodoorthoacetate

Chemical Property of triethyl iodoorthoacetate

Chemical Property:

Purity/Quality:

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Technology Process of triethyl iodoorthoacetate

There total 1 articles about triethyl iodoorthoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diiodoacetylene (624-74-8) + ethanol (64-17-5) → triethyl iodoorthoacetate (183115-34-6)

Guidance literature:

With potassium hydroxide; at 80 - 100 ℃;

Reference yield: 48.0%

2-chloro-1,1,1-triethoxyethane (51076-95-0) + triethyl iodoorthoacetate (183115-34-6) + 5'-O-trityldeoxyxylothymidine (55612-11-8) → (R)-1-[3,5-O-(2-chloro-1-ethoxyethylidene)-2-deoxy-β-D-threo-pentofurano

Guidance literature:

With hydrogenchloride; In dichloromethane; N,N-dimethyl-formamide; at 0 ℃; pH=15;

DOI:10.1016/S0040-4020(98)00654-1

Reference yield:

diethyl ether (60-29-7,927820-24-4) + triethyl iodoorthoacetate (183115-34-6) → succinic acid diethyl ester (123-25-1)

Guidance literature:

at 5 ℃;

upstream raw materials:

diiodoacetylene

ethanol

Downstream raw materials:

succinic acid diethyl ester

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