Technology Process of C31H30N2O5
There total 7 articles about C31H30N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate;
In
1,2-dimethoxyethane; water;
for 4h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -4 °C
2.1: triethylamine / dichloromethane / 3 h / -78 - 0 °C
3.1: triethylamine / N,N-dimethyl-formamide / 3 h / 70 °C
4.1: sodium hydroxide / methanol; water / 16 h / 60 °C
4.2: pH 3
5.1: hydrogenchloride / 18 h / Reflux
6.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / Inert atmosphere; Reflux
7.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 4 h / Inert atmosphere; Reflux
With
hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; lithium aluminium tetrahydride; potassium acetate; sodium carbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide;
7.1: |Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylamine / dichloromethane / 3 h / -78 - 0 °C
2.1: triethylamine / N,N-dimethyl-formamide / 3 h / 70 °C
3.1: sodium hydroxide / methanol; water / 16 h / 60 °C
3.2: pH 3
4.1: hydrogenchloride / 18 h / Reflux
5.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / Inert atmosphere; Reflux
6.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 4 h / Inert atmosphere; Reflux
With
hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; sodium carbonate; triethylamine; sodium hydroxide;
In
1,4-dioxane; methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide;
6.1: |Suzuki Coupling;