(pentaphenoxy)[4-(6-phenyl(2,2'-bipyridin)-4-yl)-phenoxy]cyclotriphosphaazene

Base Information

Chemical Name:(pentaphenoxy)[4-(6-phenyl(2,2'-bipyridin)-4-yl)-phenoxy]cyclotriphosphaazene
CAS No.:1334243-46-7
Molecular Formula:C₅₂H₃₆N₅O₆P₃
Molecular Weight:919.809
Hs Code.:

Synonyms:(pentaphenoxy)[4-(6-phenyl(2,2'-bipyridin)-4-yl)-phenoxy]cyclotriphosphaazene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (pentaphenoxy)[4-(6-phenyl(2,2'-bipyridin)-4-yl)-phenoxy]cyclotriphosphaazene

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Technology Process of (pentaphenoxy)[4-(6-phenyl(2,2'-bipyridin)-4-yl)-phenoxy]cyclotriphosphaazene

There total 1 articles about (pentaphenoxy)[4-(6-phenyl(2,2'-bipyridin)-4-yl)-phenoxy]cyclotriphosphaazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1334243-45-6
N₃P₃(biph)2(OPhbpyPh)Cl

: 108-95-2,27073-41-2
phenol

: 1334243-46-7
(pentaphenoxy)[4-(6-phenyl(2,2'-bipyridin)-4-yl)-phenoxy]cyclotriphosphaazene

Guidance literature:: phenol; With sodium hydride; In tetrahydrofuran; oil; for 0.5h;

N₃P₃(biph)2(OPhbpyPh)Cl; With tetrabutylammomium bromide; In tetrahydrofuran; oil; Reflux;
DOI:10.1002/ejic.201100341

Reference yield: 68.0%

: 14099-01-5
rhenium(I) pentacarbonyl chloride

: 1334243-46-7
(pentaphenoxy)[4-(6-phenyl(2,2'-bipyridin)-4-yl)-phenoxy]cyclotriphosphaazene

: [((pentaphenoxy)[4-(6-phenyl(2,2'-bipyridin)-4-yl)-phenoxy]cyclotriphosphazene)Re(CO)3Cl]

Guidance literature:: In toluene; mixt. of cyclotriphosphazene and rhenium complex in toluene was refluxedfor 5 h; filtered, filtrate was evapd. in vac., dissolved in CH2Cl2, filtered through celite, filtrate was crystd. with hexane, elem. anal.;
DOI:10.1021/ic902171j

Reference yield:

: 14873-63-3,15617-19-3,51921-56-3
bis(benzonitrile)dichloroplatinum(II)

: 1334243-46-7
(pentaphenoxy)[4-(6-phenyl(2,2'-bipyridin)-4-yl)-phenoxy]cyclotriphosphaazene

: 1334243-53-6
N₃P₃(2,2'-oxybiphenyl)2(4-(4-phenoxy)-6-phenyl-2,2'-bipyridine)(phenoxy)PtCl

Guidance literature:: In methanol; benzene; soln. of ligand and Pd complex (1:1) in CH3OH/benzene (1:1) refluxed overnight; filtered, washed (Et2O), dried (vac.), dissolved (CH3OH/benzene 1:1, refluxed, elem. anal.;
DOI:10.1002/ejic.201100341