C₂₇H₂₃NO₇

Base Information

Chemical Name:C₂₇H₂₃NO₇
CAS No.:1402931-81-0
Molecular Formula:C₂₇H₂₃NO₇
Molecular Weight:473.482
Hs Code.:

C<sub>27</sub>H<sub>23</sub>NO<sub>7</sub>

Synonyms:C₂₇H₂₃NO₇

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Chemical Property of C₂₇H₂₃NO₇

Chemical Property:

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Technology Process of C₂₇H₂₃NO₇

There total 14 articles about C₂₇H₂₃NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1402931-80-9
C₃₄H₂₉NO₇

: 1402931-81-0
C₂₇H₂₃NO₇

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In tetrahydrofuran; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/jm3011542

Reference yield:

: 480-40-0
5,7-dihydroxy-2-phenyl-chromen-4-one

: 1402931-81-0
C₂₇H₂₃NO₇

Guidance literature:: Multi-step reaction with 14 steps

1.1: potassium carbonate / acetone / 3 h / 60 °C / Inert atmosphere

2.1: acetone / 72 h / 40 °C / Inert atmosphere

3.1: pyridine / water; diethylene glycol / 2 h / 100 °C / Inert atmosphere; Alkaline conditions

4.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

5.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

5.2: 6 h / Inert atmosphere; Reflux

6.1: dmap; triethylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

7.1: lithium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -70 - -20 °C / Inert atmosphere

8.1: sulfuric acid; acetic acid / 8 h / 75 °C / Inert atmosphere

8.2: 2 h / 20 °C / Inert atmosphere

9.1: water; sodium hydroxide / ethanol / 1 h / 80 °C / Inert atmosphere

10.1: methanol; dichloromethane; acetonitrile / 3 h / 0 - 5 °C / Inert atmosphere; UV-irradiation

10.2: 1 h / 60 °C / Inert atmosphere

11.1: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 48 h / Inert atmosphere

12.1: LUX Cellulose-2 / methanol / Inert atmosphere; Resolution of racemate; Supercritical conditions

13.1: 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 20 h / 100 °C / Inert atmosphere

14.1: 5%-palladium/activated carbon; hydrogen / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

With pyridine; dmap; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sulfuric acid; 5%-palladium/activated carbon; water; hydrogen; sodium hydrogencarbonate; potassium carbonate; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; lithium hexamethyldisilazane; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetone; toluene; acetonitrile; diethylene glycol; 5.1: |Rubottom Oxidation / 5.2: |Rubottom Oxidation / 7.1: |Baker-Venkataraman Rearrangement;
DOI:10.1021/jm3011542

Reference yield:

: 110506-85-9
7-(benzyloxy)-5-hydroxy-2-phenyl-4H-chromen-4-one

: 1402931-81-0
C₂₇H₂₃NO₇

Guidance literature:: Multi-step reaction with 13 steps

1.1: acetone / 72 h / 40 °C / Inert atmosphere

2.1: pyridine / water; diethylene glycol / 2 h / 100 °C / Inert atmosphere; Alkaline conditions

3.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

4.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

4.2: 6 h / Inert atmosphere; Reflux

5.1: dmap; triethylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

6.1: lithium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -70 - -20 °C / Inert atmosphere

7.1: sulfuric acid; acetic acid / 8 h / 75 °C / Inert atmosphere

7.2: 2 h / 20 °C / Inert atmosphere

8.1: water; sodium hydroxide / ethanol / 1 h / 80 °C / Inert atmosphere

9.1: methanol; dichloromethane; acetonitrile / 3 h / 0 - 5 °C / Inert atmosphere; UV-irradiation

9.2: 1 h / 60 °C / Inert atmosphere

10.1: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 48 h / Inert atmosphere

11.1: LUX Cellulose-2 / methanol / Inert atmosphere; Resolution of racemate; Supercritical conditions

12.1: 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 20 h / 100 °C / Inert atmosphere

13.1: 5%-palladium/activated carbon; hydrogen / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

With pyridine; dmap; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sulfuric acid; 5%-palladium/activated carbon; water; hydrogen; sodium hydrogencarbonate; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; lithium hexamethyldisilazane; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetone; toluene; acetonitrile; diethylene glycol; 4.1: |Rubottom Oxidation / 4.2: |Rubottom Oxidation / 6.1: |Baker-Venkataraman Rearrangement;
DOI:10.1021/jm3011542