4-((3-((dimethylamino)methyl)-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)-N-hydroxybenzamide

Base Information

Chemical Name:4-((3-((dimethylamino)methyl)-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)-N-hydroxybenzamide
CAS No.:1432508-41-2
Molecular Formula:C₂₅H₂₉N₃O₃
Molecular Weight:419.524
Hs Code.:

Synonyms:4-((3-((dimethylamino)methyl)-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)-N-hydroxybenzamide

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Chemical Property of 4-((3-((dimethylamino)methyl)-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)-N-hydroxybenzamide

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Technology Process of 4-((3-((dimethylamino)methyl)-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)-N-hydroxybenzamide

There total 5 articles about 4-((3-((dimethylamino)methyl)-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)-N-hydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1432509-55-1
methyl 4-((3-((dimethylamino)methyl)-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

: 1432508-41-2
4-((3-((dimethylamino)methyl)-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)-N-hydroxybenzamide

Guidance literature:: methyl 4-((3-((dimethylamino)methyl)-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate; With hydroxylamine hydrochloride; potassium hydroxide; In methanol; for 0.166667h;

With hydroxylamine; In methanol; water; at 20 ℃; for 4h;

Reference yield:

: 1432509-06-2
methyl 4-((2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

: 1432508-41-2
4-((3-((dimethylamino)methyl)-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)-N-hydroxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / toluene / 4 h / 100 °C / Microwave irradiation

2: hydroxylamine hydrochloride; potassium hydroxide; hydroxylamine / methanol; water / 4 h / 20 °C

With hydroxylamine hydrochloride; hydroxylamine; acetic acid; potassium hydroxide; In methanol; water; toluene; 1: |Mannich Aminomethylation;

Reference yield:

: 100-63-0
phenylhydrazine

: 1432508-41-2
4-((3-((dimethylamino)methyl)-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)-N-hydroxybenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / 0.08 h / 140 °C / Microwave irradiation

2: sodium hydride / N,N-dimethyl-formamide / 6 h / 60 °C

3: acetic acid / toluene / 4 h / 100 °C / Microwave irradiation

4: hydroxylamine hydrochloride; potassium hydroxide; hydroxylamine / methanol; water / 4 h / 20 °C

With hydroxylamine hydrochloride; hydroxylamine; sodium hydride; acetic acid; trifluoroacetic acid; potassium hydroxide; In methanol; water; N,N-dimethyl-formamide; toluene; 1: |Fischer Indole Synthesis / 3: |Mannich Aminomethylation;