Pd([P(CH₃)2]2CH₂CH₂)CH₂C(CH₃)2C₆H₅P(CH₃)3⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=Pd([P(CH₃)2]2CH₂CH₂)CH₂C(CH₃)2C₆H₅P(CH₃)3B(C₆H₃(CF₃)2)4

Base Information

• Chemical Name: Pd([P(CH₃)2]2CH₂CH₂)CH₂C(CH₃)2C₆H₅P(CH₃)3⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=Pd([P(CH₃)2]2CH₂CH₂)CH₂C(CH₃)2C₆H₅P(CH₃)3B(C₆H₃(CF₃)2)4
• CAS No.: 383908-65-4
• Molecular Formula: C₁₉H₃₈P₃Pd*C₃₂H₁₂BF₂₄
• Molecular Weight: 1329.07

Synonyms:Pd([P(CH₃)2]2CH₂CH₂)CH₂C(CH₃)2C₆H₅P(CH₃)3⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=Pd([P(CH₃)2]2CH₂CH₂)CH₂C(CH₃)2C₆H₅P(CH₃)3B(C₆H₃(CF₃)2)4

Chemical Property of Pd([P(CH₃)2]2CH₂CH₂)CH₂C(CH₃)2C₆H₅P(CH₃)3⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=Pd([P(CH₃)2]2CH₂CH₂)CH₂C(CH₃)2C₆H₅P(CH₃)3B(C₆H₃(CF₃)2)4

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Technology Process of Pd([P(CH₃)2]2CH₂CH₂)CH₂C(CH₃)2C₆H₅P(CH₃)3⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=Pd([P(CH₃)2]2CH₂CH₂)CH₂C(CH₃)2C₆H₅P(CH₃)3B(C₆H₃(CF₃)2)4

There total 1 articles about Pd([P(CH₃)2]2CH₂CH₂)CH₂C(CH₃)2C₆H₅P(CH₃)3⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=Pd([P(CH₃)2]2CH₂CH₂)CH₂C(CH₃)2C₆H₅P(CH₃)3B(C₆H₃(CF₃)2)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Pd([P(CH3)2]2CH2CH2)CH2C6H4C(CH3)2 (359764-27-5) + HP(CH3)3(1+)*B(C6H3(CF3)2)4(1-)=[HP(CH3)3][B(C6H3(CF3)2)4] → Pd([P(CH3)2]2CH2CH2)CH2C(CH3)2C6H5P(CH3)3(1+)*B(C6H3(CF3)2)4(1-)=Pd([P(CH3)2]2CH2CH2)CH2C(CH3)2C6H5P(CH3)3B(C6H3(CF3)2)4 (383908-65-4)

Guidance literature:

DOI:10.1002/1521-3773(20011001)40:19<3641::AID-ANIE3641>3.0.CO;2-9

Reference yield: 60.0%

ethene (74-85-1) + Pd([P(CH3)2]2CH2CH2)CH2C(CH3)2C6H5P(CH3)3(1+)*B(C6H3(CF3)2)4(1-)=Pd([P(CH3)2]2CH2CH2)CH2C(CH3)2C6H5P(CH3)3B(C6H3(CF3)2)4 (383908-65-4) → Pd([P(CH3)2]2CH2CH2)CH2CH3P(CH3)3(1+)*B(C6H3(CF3)2)4(1-)=Pd([P(CH3)2]2CH2CH2)CH2CH3P(CH3)3B(C6H3(CF3)2)4 (383908-69-8)

Guidance literature:

Pd([P(CH₃)2]2CH₂CH₂)CH₂C₆H₅C(CH₃)2⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=Pd([P(CH₃)2]2CH₂CH₂)CH₂C₆H₅C(CH₃)2B(C₆H₃(CF₃)2)4; In diethyl ether; toluene; byproducts: styrene, isobutene, tert-butylbenzene; soln. of (P(CH3)2)2CH2CH2PdP(CH3)3CH2C(CH3)2C6H5, (P(CH3)2)2CH2CH2Pd(C6H5)CH2C(CH3)2and toluene in diethyl ester charged with C2H4 (3 bar), heated (60 °C, 24 h); soln. evapd., residue extd. (petroleum ether), filtered, recrystd. from mixt. of petroleum ether/(C2H5)2O (2:1); detd. by elem. anal., (1)H NMR,(31)P NMR; Kinetics;

DOI:10.1002/1521-3773(20011001)40:19<3641::AID-ANIE3641>3.0.CO;2-9

Reference yield:

Pd([P(CH3)2]2CH2CH2)CH2C(CH3)2C6H5P(CH3)3(1+)*B(C6H3(CF3)2)4(1-)=Pd([P(CH3)2]2CH2CH2)CH2C(CH3)2C6H5P(CH3)3B(C6H3(CF3)2)4 (383908-65-4) → Pd(C6H5)([P(CH3)2]2CH2CH2)(P(CH3)3)(1+) + isobutene (115-11-7,15220-85-6)

Guidance literature:

Pd([P(CH₃)2]2CH₂CH₂)CH₂C₆H₅C(CH₃)2⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=Pd([P(CH₃)2]2CH₂CH₂)CH₂C₆H₅C(CH₃)2B(C₆H₃(CF₃)2)4; In not given; catalytic β-C6H5 elimination react.; Kinetics;

DOI:10.1002/1521-3773(20011001)40:19<3641::AID-ANIE3641>3.0.CO;2-9

upstream raw materials:

Pd([P(CH₃)2]2CH₂CH₂)CH₂C₆H₄C(CH₃)2

Downstream raw materials:

isobutene

Pd([P(CH₃)2]2CH₂CH₂)CH₂CH₃P(CH₃)3⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=Pd([P(CH₃)2]2CH₂CH₂)CH₂CH₃P(CH₃)3B(C₆H₃(CF₃)2)4

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