(S)-2,2-Dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

Base Information

Chemical Name:(S)-2,2-Dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol
CAS No.:146903-01-7
Molecular Formula:C₃₁H₃₇NO₃
Molecular Weight:471.64
Hs Code.:

Synonyms:(S)-2,2-Dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

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Chemical Property of (S)-2,2-Dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

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Technology Process of (S)-2,2-Dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

There total 5 articles about (S)-2,2-Dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31952-16-6
2,2-dibenzyl-1,3-propanediol

: 146903-01-7
(S)-2,2-Dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / CH₂Cl₂ / Ambient temperature

2: DMSO, oxalyl chloride, diisopropylethylamine / CH₂Cl₂ / -78 deg C, 30 min then warm to room temp.

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jo00084a037

Reference yield:

: 100-39-0
benzyl bromide

: 146903-01-7
(S)-2,2-Dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃ / acetone / Heating

2: LiAlH₄ / diethyl ether / Ambient temperature

3: triethylamine / CH₂Cl₂ / Ambient temperature

4: DMSO, oxalyl chloride, diisopropylethylamine / CH₂Cl₂ / -78 deg C, 30 min then warm to room temp.

With lithium aluminium tetrahydride; oxalyl dichloride; potassium carbonate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane; acetone;
DOI:10.1021/jo00084a037

Reference yield:

: 72013-65-1
Dimethyl 2,2-dibenzylmalonate

: 146903-01-7
(S)-2,2-Dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexen-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: LiAlH₄ / diethyl ether / Ambient temperature

2: triethylamine / CH₂Cl₂ / Ambient temperature

3: DMSO, oxalyl chloride, diisopropylethylamine / CH₂Cl₂ / -78 deg C, 30 min then warm to room temp.

With lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane;
DOI:10.1021/jo00084a037