2,2'-bis(4-benzoylthio-1,3-dithiole-2-thione-5-thio)diethylsulfide

Base Information

• Chemical Name: 2,2'-bis(4-benzoylthio-1,3-dithiole-2-thione-5-thio)diethylsulfide
• CAS No.: 161090-93-3
• Molecular Formula: C₂₄H₁₈O₂S₁₁
• Molecular Weight: 691.132
• Mol file: 161090-93-3.mol

Synonyms:2,2'-bis(4-benzoylthio-1,3-dithiole-2-thione-5-thio)diethylsulfide

Chemical Property of 2,2'-bis(4-benzoylthio-1,3-dithiole-2-thione-5-thio)diethylsulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2'-bis(4-benzoylthio-1,3-dithiole-2-thione-5-thio)diethylsulfide

There total 2 articles about 2,2'-bis(4-benzoylthio-1,3-dithiole-2-thione-5-thio)diethylsulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

bis(2-bromoethyl)sulfide (7617-64-3) + caesium 4-benzoylthio-1,3-dithiole-2-thione-5-thiolate → 2,2'-bis(4-benzoylthio-1,3-dithiole-2-thione-5-thio)diethylsulfide (161090-93-3)

Guidance literature:

In ethanol; at 30 ℃; for 24h;

DOI:10.1055/s-1994-25711

Reference yield:

4,5-bis(benzoylthio)-1,3-dithiole-2-thione (68494-08-6) → 2,2'-bis(4-benzoylthio-1,3-dithiole-2-thione-5-thio)diethylsulfide (161090-93-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / caesium hydroxide hydrate / CHCl₃; methanol / 0.02 h

2: 94 percent / ethanol / 24 h / 30 °C

With cesium hydroxide; In methanol; ethanol; chloroform;

DOI:10.1055/s-1994-25711

upstream raw materials:

bis(2-bromoethyl)sulfide

4,5-bis(benzoylthio)-1,3-dithiole-2-thione