4,5-BIS(BENZOYLTHIO)-1,3-DITHIOLE-2-THIONE

Base Information

• Chemical Name: 4,5-BIS(BENZOYLTHIO)-1,3-DITHIOLE-2-THIONE
• CAS No.: 68494-08-6
• Molecular Formula: C17H10O2S5
• Molecular Weight: 406.595
• Hs Code.: 2930909090
• Mol file: 68494-08-6.mol

Synonyms:S-(5-benzoylsulfanyl-2-sulfanylidene-1,3-dithiol-4-yl) benzenecarbothioate;

Chemical Property of 4,5-BIS(BENZOYLTHIO)-1,3-DITHIOLE-2-THIONE

Chemical Property:

• Melting Point: 139-143oC
• Boiling Point: 512.1°Cat760mmHg
• Flash Point: 263.5°C
• PSA: 173.31000
• Density: 1.55g/cm³
• LogP: 6.40410
• Solubility.: almost transparency in Chloroform

Purity/Quality:

98%,99%, ^*data from raw suppliers

4,5-Bis(benzoylthio)-1,3-dithiole-2-thione ^*data from reagent suppliers

Safty Information:

• Safety Statements: 22-24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 4,5-BIS(BENZOYLTHIO)-1,3-DITHIOLE-2-THIONE

There total 9 articles about 4,5-BIS(BENZOYLTHIO)-1,3-DITHIOLE-2-THIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

benzoyl chloride (98-88-4) + bis(tetraethylammonium)bis(2-thioxo-1,3-dithiole-4,5-dithiolate)zincate (72022-68-5) → 4,5-bis(benzoylthio)-1,3-dithiole-2-thione (68494-08-6)

Guidance literature:

In acetone; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1021/ol1010467

Reference yield: 78.0%

benzoyl chloride (98-88-4) → 4,5-bis(methylthio)-1,3-dithiole-2-thione (49638-64-4) + 4,5-bis(benzoylthio)-1,3-dithiole-2-thione (68494-08-6) + 4-(benzoylthio)-5-(methylthio)-2-thioxo-1,3-dithiole (161090-91-1)

Guidance literature:

In acetone; 1.) r.t., 0.5 h, 2.) r.t., 2 h;

DOI:10.1002/chem.19970031018

Reference yield: 78.0%

methyl iodide (74-88-4) → 4,5-bis(methylthio)-1,3-dithiole-2-thione (49638-64-4) + 4,5-bis(benzoylthio)-1,3-dithiole-2-thione (68494-08-6) + 4-(benzoylthio)-5-(methylthio)-2-thioxo-1,3-dithiole (161090-91-1)

Guidance literature:

In acetone; 1.) r.t., 0.5 h, 2.) r.t., 2 h;

DOI:10.1002/chem.19970031018

upstream raw materials:

carbon disulfide

benzoyl chloride

methyl iodide

bis(tetraethylammonium)bis(2-thioxo-1,3-dithiole-4,5-dithiolate)zincate

Downstream raw materials:

1,3,4,6-tetrathiapentalene-2-thione

10aH-1,3,4,5-Tetrathia-cyclohepta[e]indene-2-thione

benzoic acid

6-Phenyl-10aH-1,3,4,5-tetrathia-cyclohepta[e]indene-2-thione

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