-<2-<<2-<(3-bromo-1-oxopropyl)amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester

Base Information

• Chemical Name: -<2-<<2-<(3-bromo-1-oxopropyl)amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester
• CAS No.: 141956-49-2
• Molecular Formula: C₃₄H₄₁BrN₄O₄
• Molecular Weight: 649.628

Synonyms:-<2-<<2-<(3-bromo-1-oxopropyl)amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester

Chemical Property of -<2-<<2-<(3-bromo-1-oxopropyl)amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester

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Technology Process of -<2-<<2-<(3-bromo-1-oxopropyl)amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester

There total 1 articles about -<2-<<2-<(3-bromo-1-oxopropyl)amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Bromopropionic acid (590-92-1) + tricyclo<3.3.1.13,7>dec-2-yl *,R*)>-<2-<(2-amino-2-phenylethyl)amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamate (130406-64-3) → -<2-<<2-<(3-bromo-1-oxopropyl)amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.13,7>dec-2-yl ester (141956-49-2)

Guidance literature:

With 2,3,4,5,6-pentafluorophenol; dicyclohexyl-carbodiimide; Yield given. Multistep reaction; 1.) EtOAc, RT, 2 h, 2.) EtOAc, RT, overnight;

DOI:10.1021/jm00092a007

Reference yield: 55.0%

Diethyl methylphosphonate (683-08-9) + -<2-<<2-<(3-bromo-1-oxopropyl)amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.13,7>dec-2-yl ester (141956-49-2) → -<2-<<2-<<3-(ethoxymethylphosphinyl)-1-oxopropyl>amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.13,7>dec-2-yl ester (141956-51-6,142035-19-6)

Guidance literature:

In toluene; at 110 ℃; for 2h;

DOI:10.1021/jm00092a007

Reference yield: 52.0%

-<2-<<2-<(3-bromo-1-oxopropyl)amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.13,7>dec-2-yl ester (141956-49-2) → -<1-(1H-indol-3-ylmethyl)-1-methyl-2-oxo-2-<<2-<(1-oxo-3-sulfopropyl)amino>-2-phenylethyl>amino>ethyl>carbamic acid tricyclo<3.3.1.13,7>dec-2-yl ester monosodium salt (141980-80-5)

Guidance literature:

With sodium sulfite; In ethanol; for 2h; Heating;

DOI:10.1021/jm00092a007

upstream raw materials:

3-Bromopropionic acid

tricyclo<3.3.1.1^3,7>dec-2-yl *,R^*)>-<2-<(2-amino-2-phenylethyl)amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamate

Downstream raw materials:

-<2-<<2-<<3-(ethoxymethylphosphinyl)-1-oxopropyl>amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester

-<1-(1H-indol-3-ylmethyl)-1-methyl-2-oxo-2-<<2-<(1-oxo-3-sulfopropyl)amino>-2-phenylethyl>amino>ethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester monosodium salt

-<2-<<2-<<3-(hydroxymethylphosphinyl)-1-oxopropyl>amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester

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