4-ethylpent-4-enyloxymethylbenzene

Base Information

Chemical Name:4-ethylpent-4-enyloxymethylbenzene
CAS No.:528607-23-0
Molecular Formula:C₁₄H₂₀O
Molecular Weight:204.312
Hs Code.:

Synonyms:4-ethylpent-4-enyloxymethylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-ethylpent-4-enyloxymethylbenzene

Chemical Property:

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Technology Process of 4-ethylpent-4-enyloxymethylbenzene

There total 3 articles about 4-ethylpent-4-enyloxymethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 59518-08-0
4-ethylpent-4-en-1-ol

: 100-39-0
benzyl bromide

: 528607-23-0
4-ethylpent-4-enyloxymethylbenzene

Guidance literature:: With sodium hydride; sodium iodide; In N,N-dimethyl-formamide; at 18 ℃; for 18h;
DOI:10.1039/b209992f

Reference yield:

: 13064-28-3
methyl 4-nitrohexanoate

: 528607-23-0
4-ethylpent-4-enyloxymethylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 95 percent / aq. NaHCO₃; K₂CO₃; Oxone / acetone / 29 h / 18 °C

2.1: NaHMDS / tetrahydrofuran / 1.5 h / 18 °C

2.2: 30 percent / tetrahydrofuran / 15 h / 18 °C

3.1: 57 percent / LiAlH₄ / diethyl ether / 1.5 h

4.1: 70 percent / NaH; NaI / dimethylformamide / 18 h / 18 °C

With Oxone; lithium aluminium tetrahydride; sodium hexamethyldisilazane; sodium hydride; sodium hydrogencarbonate; potassium carbonate; sodium iodide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; acetone; 1.1: Nef reaction / 2.2: Wittig reaction;
DOI:10.1039/b209992f

Reference yield:

: 2955-62-6
methyl 4-oxohexanoate

: 528607-23-0
4-ethylpent-4-enyloxymethylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaHMDS / tetrahydrofuran / 1.5 h / 18 °C

1.2: 30 percent / tetrahydrofuran / 15 h / 18 °C

2.1: 57 percent / LiAlH₄ / diethyl ether / 1.5 h

3.1: 70 percent / NaH; NaI / dimethylformamide / 18 h / 18 °C

With lithium aluminium tetrahydride; sodium hexamethyldisilazane; sodium hydride; sodium iodide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; 1.2: Wittig reaction;
DOI:10.1039/b209992f