Fe(C₅H₅)(CO)P(C₆H₅)3CCH

Base Information

• Chemical Name: Fe(C₅H₅)(CO)P(C₆H₅)3CCH
• CAS No.: 80642-59-7
• Molecular Formula: C₂₆H₂₁FeOP
• Molecular Weight: 436.273

Synonyms:Fe(C₅H₅)(CO)P(C₆H₅)3CCH

Chemical Property of Fe(C₅H₅)(CO)P(C₆H₅)3CCH

Chemical Property:

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Technology Process of Fe(C₅H₅)(CO)P(C₆H₅)3CCH

There total 4 articles about Fe(C₅H₅)(CO)P(C₆H₅)3CCH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

{Cp(CO)(Ph3P)FeCCH2}BF4 + dimethyl amine (124-40-3) → Fe(C5H5)(CO)P(C6H5)3CCH (80642-59-7)

Guidance literature:

In neat (no solvent); The mixt. of reagents were stirred at -116°C for 2 h (N2 atm.);; evapd., chromd. in silica gel column with Et2O, acetone; recrystd. fromtoluene-hexane;;

Reference yield: 77.0%

{Cp(CO)(Ph3P)FeCCH2}BF4 + dimethyl amine (124-40-3) → acetyl carbonyl cyclopentadienyl triphenylphosphine iron + Fe(C5H5)(CO)P(C6H5)3CCH (80642-59-7) + C5H5Fe(CO)P(C6H5)3C(N(CH3)2)CH3(1+)*BF4(1-) (80662-30-2)

Guidance literature:

In neat (no solvent); the mixt. of reagents was stirred for 1 h (N2 atm.);; evapd., chromd. in silica gel column with Et2O, acetone; recrystd. fromCH2Cl2-Et2O;

Reference yield: 75.0%

{Cp(CO)(Ph3P)FeCCH2}BF4 → acetyl carbonyl cyclopentadienyl triphenylphosphine iron + Fe(C5H5)(CO)P(C6H5)3CCH (80642-59-7) + (C5H5)Fe(C(NHCH3)CH3)(CO)(P(C6H5)3)(1+)*BF4(1-) = [(C5H5)Fe(C(NHCH3)CH3)(CO)(P(C6H5)3)]BF4 (80662-48-2)

Guidance literature:

With methylamine; In neat (no solvent); MeNH2 was condensed on to complex at -196°C, the mixt. was warmed to -24°C and stirred for 1 h (N2 atm.);; evapd., chromd. in silica gel column with Et2O-CH2Cl2; recrystd.;

upstream raw materials:

dimethyl amine

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