Technology Process of C16H13FN2O4
There total 6 articles about C16H13FN2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) thionyl chloride, 2.) aluminum chloride / 1.) 1,2-dichloroethane, from 65 to 70 deg C, 0.75 h, 2.) 1,2-dichloroethane, 42 deg C, 0.75 h
2: 72 percent / hydroxylamine hydrochloride, sodium acetate / ethanol; H2O
3: 88 percent / pyridine
With
pyridine; aluminium trichloride; thionyl chloride; hydroxylamine hydrochloride; sodium acetate;
In
ethanol; water;
DOI:10.1021/jm00346a004
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) thionyl chloride, 2.) aluminum chloride / 1.) 1,2-dichloroethane, from 65 to 70 deg C, 0.75 h, 2.) 1,2-dichloroethane, 42 deg C, 0.75 h
2: 72 percent / hydroxylamine hydrochloride, sodium acetate / ethanol; H2O
3: 88 percent / pyridine
With
pyridine; aluminium trichloride; thionyl chloride; hydroxylamine hydrochloride; sodium acetate;
In
ethanol; water;
DOI:10.1021/jm00346a004