5-(4-Methoxy-phenyl)-4-{[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazol-3-one

Base Information

Chemical Name:5-(4-Methoxy-phenyl)-4-{[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazol-3-one
CAS No.:86268-12-4
Molecular Formula:C₁₇H₁₆N₄O₃
Molecular Weight:324.339
Hs Code.:

Synonyms:5-(4-Methoxy-phenyl)-4-{[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazol-3-one

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Chemical Property of 5-(4-Methoxy-phenyl)-4-{[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazol-3-one

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 5-(4-Methoxy-phenyl)-4-{[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazol-3-one

There total 4 articles about 5-(4-Methoxy-phenyl)-4-{[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazol-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 6638-56-8
2,2'-bis[(4-methoxyphenyl)methylene]carbonic dihydrazide

: 2299-73-2,41097-47-6
N,N-bis(4-methoxybenzylidene)hydrazine

: 86268-12-4
5-(4-Methoxy-phenyl)-4-{[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazol-3-one

Guidance literature:: With lead dioxide; In N,N-dimethyl-formamide; at 125 - 130 ℃; for 2.5h;

Reference yield: 70.0%

: 123-11-5
4-methoxy-benzaldehyde

: 70249-92-2
4-amino-5-(4-methoxy-phenyl)-2,4-dihydro-[1,2,4]triazol-3-one

: 86268-12-4
5-(4-Methoxy-phenyl)-4-{[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazol-3-one

Guidance literature:: With sodium acetate; In ethanol; for 4h; Heating;

Reference yield:

: 3290-99-1
4-methoxybenzoic acid hydrazide

: 86268-12-4
5-(4-Methoxy-phenyl)-4-{[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazol-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / ethanol

2: 60 percent / NH₂NH₂*H₂O / 8 h / 140 - 160 °C

3: 70 percent / NaOAc / ethanol / 4 h / Heating

With potassium hydroxide; sodium acetate; hydrazine hydrate; In ethanol;