(2S,3S)-3-Amino-2-(2,4-dichloro-phenyl)-1-[1,2,4]triazol-1-yl-butan-2-ol

Base Information

Chemical Name:(2S,3S)-3-Amino-2-(2,4-dichloro-phenyl)-1-[1,2,4]triazol-1-yl-butan-2-ol
CAS No.:132563-80-5
Molecular Formula:C₁₂H₁₄Cl₂N₄O
Molecular Weight:301.175
Hs Code.:

Synonyms:(2S,3S)-3-Amino-2-(2,4-dichloro-phenyl)-1-[1,2,4]triazol-1-yl-butan-2-ol

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Chemical Property of (2S,3S)-3-Amino-2-(2,4-dichloro-phenyl)-1-[1,2,4]triazol-1-yl-butan-2-ol

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Technology Process of (2S,3S)-3-Amino-2-(2,4-dichloro-phenyl)-1-[1,2,4]triazol-1-yl-butan-2-ol

There total 5 articles about (2S,3S)-3-Amino-2-(2,4-dichloro-phenyl)-1-[1,2,4]triazol-1-yl-butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: (2S,3S)-3-Azido-2-(2,4-dichloro-phenyl)-1-[1,2,4]triazol-1-yl-butan-2-ol

: 126916-51-6,127181-91-3,132563-80-5,141847-35-0
(2R*,3R*)-3-Amino-2-(2,4-dichlorophenyl)-1-(1H-1,2,4-triazol-1-yl)-2-butanol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 1h;
DOI:10.1248/cpb.38.2476

Reference yield: 100.0%

: 132563-75-8
(2S,3S)-3-Azido-2-(2,4-dichloro-phenyl)-1-[1,2,4]triazol-1-yl-butan-2-ol

: 132563-80-5
(2S,3S)-3-Amino-2-(2,4-dichloro-phenyl)-1-[1,2,4]triazol-1-yl-butan-2-ol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 1h;
DOI:10.1248/cpb.38.2476

Reference yield:

: 126916-49-2,127181-87-7,132563-72-5
(2R,3R)-2-(2,4-Dichloro-phenyl)-1-[1,2,4]triazol-1-yl-butane-2,3-diol

: 126916-51-6,127181-91-3,132563-80-5,141847-35-0
(2R*,3R*)-3-Amino-2-(2,4-dichlorophenyl)-1-(1H-1,2,4-triazol-1-yl)-2-butanol

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / pyridine / 2 h / Ambient temperature

2: 75 percent / NaN₃, NH₄Cl / dimethylformamide / 15 h / 115 °C

3: 100 percent / H₂ / 10percent Pd/C / ethanol / 1 h

With pyridine; sodium azide; hydrogen; ammonium chloride; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.38.2476