phenylmethyl methyl({3-nitro-4-[(2,2,2-trifluoroethyl)amino]phenyl}sulfonyl)carbamate

Base Information

Chemical Name:phenylmethyl methyl({3-nitro-4-[(2,2,2-trifluoroethyl)amino]phenyl}sulfonyl)carbamate
CAS No.:1301761-67-0
Molecular Formula:C₁₇H₁₆F₃N₃O₆S
Molecular Weight:447.392
Hs Code.:

Synonyms:phenylmethyl methyl({3-nitro-4-[(2,2,2-trifluoroethyl)amino]phenyl}sulfonyl)carbamate

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Chemical Property of phenylmethyl methyl({3-nitro-4-[(2,2,2-trifluoroethyl)amino]phenyl}sulfonyl)carbamate

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Technology Process of phenylmethyl methyl({3-nitro-4-[(2,2,2-trifluoroethyl)amino]phenyl}sulfonyl)carbamate

There total 4 articles about phenylmethyl methyl({3-nitro-4-[(2,2,2-trifluoroethyl)amino]phenyl}sulfonyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 753-90-2
trifluoroethylamine

: 1301761-66-9
phenylmethyl N-[(4-fluoro-3-nitrophenyl)sulfonyl]-N-methylcarbamate

: 1301761-67-0
phenylmethyl methyl({3-nitro-4-[(2,2,2-trifluoroethyl)amino]phenyl}sulfonyl)carbamate

Guidance literature:: In tetrahydrofuran; at 25 ℃; for 20h;

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1301761-67-0
phenylmethyl methyl({3-nitro-4-[(2,2,2-trifluoroethyl)amino]phenyl}sulfonyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: chlorosulfonic acid / 18 h / 65 - 100 °C

2: triethylamine / tetrahydrofuran / 1 h / -35 °C

3: triethylamine / tetrahydrofuran / 5 h / 25 °C

4: tetrahydrofuran / 20 h / 25 °C

With chlorosulfonic acid; triethylamine; In tetrahydrofuran;

Reference yield:

: 6668-56-0
4-fluoro-3-nitrobenzene-1-sulfonyl chloride

: 1301761-67-0
phenylmethyl methyl({3-nitro-4-[(2,2,2-trifluoroethyl)amino]phenyl}sulfonyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 1 h / -35 °C

2: triethylamine / tetrahydrofuran / 5 h / 25 °C

3: tetrahydrofuran / 20 h / 25 °C

With triethylamine; In tetrahydrofuran;