phenylmethyl methyl({4-[methyl(2,2,2-trifluoroethyl)amino]-3-nitrophenyl}sulfonyl)carbamate

Base Information

Chemical Name:phenylmethyl methyl({4-[methyl(2,2,2-trifluoroethyl)amino]-3-nitrophenyl}sulfonyl)carbamate
CAS No.:1301761-68-1
Molecular Formula:C₁₈H₁₈F₃N₃O₆S
Molecular Weight:461.419
Hs Code.:

Synonyms:phenylmethyl methyl({4-[methyl(2,2,2-trifluoroethyl)amino]-3-nitrophenyl}sulfonyl)carbamate

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Chemical Property of phenylmethyl methyl({4-[methyl(2,2,2-trifluoroethyl)amino]-3-nitrophenyl}sulfonyl)carbamate

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Technology Process of phenylmethyl methyl({4-[methyl(2,2,2-trifluoroethyl)amino]-3-nitrophenyl}sulfonyl)carbamate

There total 5 articles about phenylmethyl methyl({4-[methyl(2,2,2-trifluoroethyl)amino]-3-nitrophenyl}sulfonyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1301761-67-0
phenylmethyl methyl({3-nitro-4-[(2,2,2-trifluoroethyl)amino]phenyl}sulfonyl)carbamate

: 74-88-4
methyl iodide

: 1301761-68-1
phenylmethyl methyl({4-[methyl(2,2,2-trifluoroethyl)amino]-3-nitrophenyl}sulfonyl)carbamate

Guidance literature:: phenylmethyl methyl({3-nitro-4-[(2,2,2-trifluoroethyl)amino]phenyl}sulfonyl)carbamate; With sodium hydride; In N,N-dimethyl-formamide; at 25 ℃; for 0.0333333h;

methyl iodide; In N,N-dimethyl-formamide; at 25 ℃; for 1h;

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1301761-68-1
phenylmethyl methyl({4-[methyl(2,2,2-trifluoroethyl)amino]-3-nitrophenyl}sulfonyl)carbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: chlorosulfonic acid / 18 h / 65 - 100 °C

2.1: triethylamine / tetrahydrofuran / 1 h / -35 °C

3.1: triethylamine / tetrahydrofuran / 5 h / 25 °C

4.1: tetrahydrofuran / 20 h / 25 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0.03 h / 25 °C

5.2: 1 h / 25 °C

With chlorosulfonic acid; sodium hydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 1041598-53-1
4-fluoro-N-methyl-3-nitrobenzenesulfonamide

: 1301761-68-1
phenylmethyl methyl({4-[methyl(2,2,2-trifluoroethyl)amino]-3-nitrophenyl}sulfonyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran / 5 h / 25 °C

2.1: tetrahydrofuran / 20 h / 25 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.03 h / 25 °C

3.2: 1 h / 25 °C

With sodium hydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;