C₁₅H₂₄O₂

Base Information

• Chemical Name: C₁₅H₂₄O₂
• CAS No.: 1016669-27-4
• Molecular Formula: C₁₅H₂₄O₂
• Molecular Weight: 236.354
• Mol file: 1016669-27-4.mol

Synonyms:C₁₅H₂₄O₂

Chemical Property of C₁₅H₂₄O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₅H₂₄O₂

There total 2 articles about C₁₅H₂₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

(+/-)-4-cyclohexyl-but-3-yn-2-ol (65199-70-4) + pivaloyl chloride (3282-30-2) → C15H24O2 (1016669-27-4)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/ja800001h

Reference yield:

2-cyclohexylacetylene (931-48-6) → C15H24O2 (1016669-27-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C

1.2: -78 - 20 °C

2.1: triethylamine; dmap / dichloromethane / 2 h / 20 °C

With dmap; n-butyllithium; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1002/anie.201302402

Reference yield:

C15H24O2 (1016669-27-4) → C15H24O2 (1016669-40-1) + C15H24O2

Guidance literature:

iPrAuNTf₂; In 1,2-dichloro-ethane; at 80 ℃; for 10h; Title compound not separated from byproducts.;

DOI:10.1021/ja800001h

upstream raw materials:

(+/-)-4-cyclohexyl-but-3-yn-2-ol

pivaloyl chloride

2-cyclohexylacetylene

Downstream raw materials:

C₁₅H₂₄O₂