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4,4,5,5,-tetramethyl-2,2,2-triphenyl-1,3,2λ(5)-dioxastibolane

Base Information Edit
  • Chemical Name:4,4,5,5,-tetramethyl-2,2,2-triphenyl-1,3,2λ(5)-dioxastibolane
  • CAS No.:71617-05-5
  • Molecular Formula:C24H27O2Sb
  • Molecular Weight:469.227
  • Hs Code.:
  • Mol file:71617-05-5.mol
4,4,5,5,-tetramethyl-2,2,2-triphenyl-1,3,2λ(5)-dioxastibolane

Synonyms:4,4,5,5,-tetramethyl-2,2,2-triphenyl-1,3,2λ(5)-dioxastibolane

Suppliers and Price of 4,4,5,5,-tetramethyl-2,2,2-triphenyl-1,3,2λ(5)-dioxastibolane
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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 4,4,5,5,-tetramethyl-2,2,2-triphenyl-1,3,2λ(5)-dioxastibolane Edit
Chemical Property:
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Technology Process of 4,4,5,5,-tetramethyl-2,2,2-triphenyl-1,3,2λ(5)-dioxastibolane

There total 2 articles about 4,4,5,5,-tetramethyl-2,2,2-triphenyl-1,3,2λ(5)-dioxastibolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium sulfate; In 1,4-dioxane; soln. of peroxo compd. slow. addn. (0-5°C, stirring) to soln. of Sb-compd. and diol with anhydrous sulfate; after 30 min solvent removal, solid residue recrystn. (ethanol);
Guidance literature:
Triphenylstibin, Dioxethan (1);
DOI:10.1021/jo01338a008
Guidance literature:
byproducts: acetone; at 260 to 270°C;
upstream raw materials:

2,3-dimethyl-2,3-butane diol

triphenylantimony

Downstream raw materials:

triphenylantimony

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