7-chloro-8-methoxy-3-butyl-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

Base Information

Chemical Name:7-chloro-8-methoxy-3-butyl-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine
CAS No.:171285-69-1
Molecular Formula:C₂₁H₂₆ClNO
Molecular Weight:343.897
Hs Code.:

Synonyms:7-chloro-8-methoxy-3-butyl-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

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Chemical Property of 7-chloro-8-methoxy-3-butyl-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

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Technology Process of 7-chloro-8-methoxy-3-butyl-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

There total 4 articles about 7-chloro-8-methoxy-3-butyl-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 109-65-9
1-bromo-butane

: 73445-60-0
(+/-)-7-chloro-8-methoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

: 171285-69-1
7-chloro-8-methoxy-3-butyl-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

Guidance literature:: With potassium carbonate; In dichloromethane; water; N,N-dimethyl-formamide; for 18h;
DOI:10.1021/jm00021a018

Reference yield:

: 7569-87-1
3-chloro-4-methoxyphenethylamine

: 171285-69-1
7-chloro-8-methoxy-3-butyl-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / tetrahydrofuran / 18 h / Heating

2: 95 percent / 99percent CF₃COOH, 99percent CH₃SO₃H / 18 h / Heating

3: 70 percent / K₂CO₃ / dimethylformamide; H₂O; CH₂Cl₂ / 18 h

With methanesulfonic acid; potassium carbonate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00021a018

Reference yield:

: 73445-59-7
2-amino>-1-phenylethanol

: 171285-69-1
7-chloro-8-methoxy-3-butyl-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 99percent CF₃COOH, 99percent CH₃SO₃H / 18 h / Heating

2: 70 percent / K₂CO₃ / dimethylformamide; H₂O; CH₂Cl₂ / 18 h

With methanesulfonic acid; potassium carbonate; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00021a018