Technology Process of (+/-)-7-chloro-8-methoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine
There total 4 articles about (+/-)-7-chloro-8-methoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanesulfonic acid; trifluoroacetic acid;
for 18h;
Heating;
DOI:10.1021/jm00021a018
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 50 percent / tetrahydrofuran / 18 h / Heating
2: 95 percent / 99percent CF3COOH, 99percent CH3SO3H / 18 h / Heating
With
methanesulfonic acid; trifluoroacetic acid;
In
tetrahydrofuran;
DOI:10.1021/jm00021a018
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 90 percent / LiAlH4, 98percent H2SO4 / tetrahydrofuran / 1 h / Ambient temperature
2: 50 percent / tetrahydrofuran / 18 h / Heating
3: 95 percent / 99percent CF3COOH, 99percent CH3SO3H / 18 h / Heating
With
lithium aluminium tetrahydride; methanesulfonic acid; sulfuric acid; trifluoroacetic acid;
In
tetrahydrofuran;
DOI:10.1021/jm00021a018
