cyclohexanespiro-2-(5-aza-4-phenyl-3-thiabicyclo<4.4.0>deca-1(6),4-diene)

Base Information

Chemical Name:cyclohexanespiro-2-(5-aza-4-phenyl-3-thiabicyclo<4.4.0>deca-1(6),4-diene)
CAS No.:115464-12-5
Molecular Formula:C₁₉H₂₃NS
Molecular Weight:297.464
Hs Code.:

Synonyms:cyclohexanespiro-2-(5-aza-4-phenyl-3-thiabicyclo<4.4.0>deca-1(6),4-diene)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclohexanespiro-2-(5-aza-4-phenyl-3-thiabicyclo<4.4.0>deca-1(6),4-diene)

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Technology Process of cyclohexanespiro-2-(5-aza-4-phenyl-3-thiabicyclo<4.4.0>deca-1(6),4-diene)

There total 4 articles about cyclohexanespiro-2-(5-aza-4-phenyl-3-thiabicyclo<4.4.0>deca-1(6),4-diene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 105983-29-7
1-benzamido-2-(cyclohex-1-enyl)cyclohex-1-ene

: 115464-12-5
cyclohexanespiro-2-(5-aza-4-phenyl-3-thiabicyclo<4.4.0>deca-1(6),4-diene)

Guidance literature:: With Lawessons reagent; In toluene; at 100 ℃; for 2h;
DOI:10.1021/jo00255a035

Reference yield: 63.0%

: 1502-22-3
2-(1-cyclohexenyl)cyclohexanone

: 2227-79-4
benzenecarbothioamide

: 115464-12-5
cyclohexanespiro-2-(5-aza-4-phenyl-3-thiabicyclo<4.4.0>deca-1(6),4-diene)

Guidance literature:: With naphthalene-2-sulfonate; In toluene; for 24h; Heating;
DOI:10.1021/jo00255a035

Reference yield:

: 1502-22-3
2-(1-cyclohexenyl)cyclohexanone

: 115464-12-5
cyclohexanespiro-2-(5-aza-4-phenyl-3-thiabicyclo<4.4.0>deca-1(6),4-diene)

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / β-naphthalenesulfonic acid / toluene / 24 h / Heating

2: 89 percent / (CH₃OC₆H₄)2P₂S₄ Lawesson reagent / toluene / 2 h / 100 °C

With Lawessons reagent; naphthalene-2-sulfonate; In toluene;
DOI:10.1021/jo00255a035