C₃₅H₂₆F₆INO₂S₂

Base Information

• Chemical Name: C₃₅H₂₆F₆INO₂S₂
• CAS No.: 1388722-82-4
• Molecular Formula: C₃₅H₂₆F₆INO₂S₂
• Molecular Weight: 797.624
• Mol file: 1388722-82-4.mol

Synonyms:C₃₅H₂₆F₆INO₂S₂

Chemical Property of C₃₅H₂₆F₆INO₂S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₂₆F₆INO₂S₂

There total 5 articles about C₃₅H₂₆F₆INO₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

4-methoxy-N-(4-methoxyphenyl)-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]benzenamine (875667-84-8) + 3-(3,3,4,4,5,5-hexafluoro-2-(5-iodo-2-methylthiophen-3-yl)cyclopent-1-enyl)-5-iodo-2-methylthiophene → C35H26F6INO2S2 (1388722-82-4)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; at 80 ℃; Inert atmosphere;

DOI:10.1021/jo301083a

Reference yield:

4-bromo-N,N-bis-(4-methoxyphenyl)aniline (194416-45-0) → C35H26F6INO2S2 (1388722-82-4)

Guidance literature:

Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; sodium acetate / PEG₆₀₀ / 85 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 80 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium acetate; sodium carbonate; In tetrahydrofuran; PEG₆₀₀; water;

DOI:10.1021/jo301083a

Reference yield:

para-iodoanisole (696-62-8) → C35H26F6INO2S2 (1388722-82-4)

Guidance literature:

Multi-step reaction with 3 steps

1: copper(l) iodide; 1,10-Phenanthroline; potassium hydroxide / toluene / 72 h / 90 °C

2: bis-triphenylphosphine-palladium(II) chloride; sodium acetate / PEG₆₀₀ / 85 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 80 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,10-Phenanthroline; sodium acetate; sodium carbonate; potassium hydroxide; In tetrahydrofuran; PEG₆₀₀; water; toluene;

DOI:10.1021/jo301083a

upstream raw materials:

3,5-dibromo-2-methylthiophene

4-methoxy-N-(4-methoxyphenyl)-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]benzenamine

para-iodoanisole

(Z)-3,3,4,4,5,5-hexafluorocyclopent-1-ene

Downstream raw materials:

C₅₉H₅₂BF₆NO₂S₂