2',4',4''-tri-O-acetyl-20-deoxo-3-O-(4-O-phenoxyacetyl-α-L-cladinosyl)desmycosin

Base Information

Chemical Name:2',4',4''-tri-O-acetyl-20-deoxo-3-O-(4-O-phenoxyacetyl-α-L-cladinosyl)desmycosin
CAS No.:121230-91-9
Molecular Formula:C₆₁H₉₃NO₂₁
Molecular Weight:1176.4
Hs Code.:

Synonyms:2',4',4''-tri-O-acetyl-20-deoxo-3-O-(4-O-phenoxyacetyl-α-L-cladinosyl)desmycosin

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Chemical Property of 2',4',4''-tri-O-acetyl-20-deoxo-3-O-(4-O-phenoxyacetyl-α-L-cladinosyl)desmycosin

Chemical Property:

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Technology Process of 2',4',4''-tri-O-acetyl-20-deoxo-3-O-(4-O-phenoxyacetyl-α-L-cladinosyl)desmycosin

There total 7 articles about 2',4',4''-tri-O-acetyl-20-deoxo-3-O-(4-O-phenoxyacetyl-α-L-cladinosyl)desmycosin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 121203-07-4
2',4',4''-tri-O-acetyl-20-deoxodesmycosin

: 121203-06-3
1-deoxy-4-O-phenoxyacetyl-1-(2-pyridylthio)-α-cladinoside

: 121203-17-6
1-deoxy-4-O-phenoxyacetyl-1-(2-pyridylthio)-β-cladinoside

: 121230-91-9
2',4',4''-tri-O-acetyl-20-deoxo-3-O-(4-O-phenoxyacetyl-α-L-cladinosyl)desmycosin

Guidance literature:: With silver trifluoromethanesulfonate; In acetonitrile; at 25 ℃; for 21h;

Reference yield:

: 18423-89-7,19231-36-8,26548-40-3,119241-37-1,138232-54-9
L-cladinose

: 121230-91-9
2',4',4''-tri-O-acetyl-20-deoxo-3-O-(4-O-phenoxyacetyl-α-L-cladinosyl)desmycosin

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

2: 72 percent / 0.1M aq. hydrochloric acid / acetonitrile / 18 h / 25 °C

3: tributylphosphine / CH₂Cl₂ / 20 h / 14 °C

4: 52 percent / silver trifluoromethanesulphonate / acetonitrile / 21 h / 25 °C

With pyridine; hydrogenchloride; tributylphosphine; silver trifluoromethanesulfonate; In dichloromethane; acetonitrile;

Reference yield:

: 14316-61-1
phenoxyacetic anhydride

: 121230-91-9
2',4',4''-tri-O-acetyl-20-deoxo-3-O-(4-O-phenoxyacetyl-α-L-cladinosyl)desmycosin

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

2: 72 percent / 0.1M aq. hydrochloric acid / acetonitrile / 18 h / 25 °C

3: tributylphosphine / CH₂Cl₂ / 20 h / 14 °C

4: 52 percent / silver trifluoromethanesulphonate / acetonitrile / 21 h / 25 °C

With pyridine; hydrogenchloride; tributylphosphine; silver trifluoromethanesulfonate; In dichloromethane; acetonitrile;