2-{[(2S,3S)-3-(2-ethoxyphenoxy)-2-hydroxy-3-phenylpropyl]amino}ethyl hydrogen sulfate

Base Information

Chemical Name:2-{[(2S,3S)-3-(2-ethoxyphenoxy)-2-hydroxy-3-phenylpropyl]amino}ethyl hydrogen sulfate
CAS No.:1250978-71-2
Molecular Formula:C₁₉H₂₅NO₇S
Molecular Weight:411.476
Hs Code.:

Synonyms:2-{[(2S,3S)-3-(2-ethoxyphenoxy)-2-hydroxy-3-phenylpropyl]amino}ethyl hydrogen sulfate

Suppliers and Price of 2-{[(2S,3S)-3-(2-ethoxyphenoxy)-2-hydroxy-3-phenylpropyl]amino}ethyl hydrogen sulfate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-{[(2S,3S)-3-(2-ethoxyphenoxy)-2-hydroxy-3-phenylpropyl]amino}ethyl hydrogen sulfate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-{[(2S,3S)-3-(2-ethoxyphenoxy)-2-hydroxy-3-phenylpropyl]amino}ethyl hydrogen sulfate

There total 17 articles about 2-{[(2S,3S)-3-(2-ethoxyphenoxy)-2-hydroxy-3-phenylpropyl]amino}ethyl hydrogen sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 926-39-6
sulfuric acid mono-(2-amino-ethyl ester)

: 98769-72-3,98819-72-8
(-)-(2S,3S)-3-(2-ethoxyphenoxy)-3-phenylpropene-1,2-epoxide

: 1250978-71-2
2-{[(2S,3S)-3-(2-ethoxyphenoxy)-2-hydroxy-3-phenylpropyl]amino}ethyl hydrogen sulfate

: 1250978-88-1
C₃₆H₄₃NO₁₀S

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In ethanol; toluene;
DOI:10.1021/op200181f

Reference yield: 78.0%

: 926-39-6
sulfuric acid mono-(2-amino-ethyl ester)

: 98769-72-3,98819-72-8
(-)-(2S,3S)-3-(2-ethoxyphenoxy)-3-phenylpropene-1,2-epoxide

: 1250978-71-2
2-{[(2S,3S)-3-(2-ethoxyphenoxy)-2-hydroxy-3-phenylpropyl]amino}ethyl hydrogen sulfate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; Inert atmosphere;
DOI:10.1039/c3ob40853a

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 1250978-71-2
2-{[(2S,3S)-3-(2-ethoxyphenoxy)-2-hydroxy-3-phenylpropyl]amino}ethyl hydrogen sulfate

Guidance literature:: Multi-step reaction with 5 steps

2: Novozymes CaL B / toluene / 17 h / 30 °C

3: triethylamine / toluene / 3 h

4: methyl tributylammonium chloride; sodium hydroxide / water / 3.5 h

5: 1,8-diazabicyclo[5.4.0]undec-7-ene / ethanol; toluene / 65 - 70 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; methyl tributylammonium chloride; sodium hydroxide; In ethanol; water; toluene; 1: Sharpless epoxidation;
DOI:10.1039/c1gc15921f