6-[(diphenylphosphanyl)methoxy]-4,8-di-tert-butyl-2,10-dimethoxy-5,7-dioxa-6-phosphadibenzo[a,c]cycloheptene

Base Information

Chemical Name:6-[(diphenylphosphanyl)methoxy]-4,8-di-tert-butyl-2,10-dimethoxy-5,7-dioxa-6-phosphadibenzo[a,c]cycloheptene
CAS No.:425429-85-2
Molecular Formula:C₃₅H₄₀O₅P₂
Molecular Weight:602.647
Hs Code.:

Synonyms:6-[(diphenylphosphanyl)methoxy]-4,8-di-tert-butyl-2,10-dimethoxy-5,7-dioxa-6-phosphadibenzo[a,c]cycloheptene

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Chemical Property of 6-[(diphenylphosphanyl)methoxy]-4,8-di-tert-butyl-2,10-dimethoxy-5,7-dioxa-6-phosphadibenzo[a,c]cycloheptene

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Technology Process of 6-[(diphenylphosphanyl)methoxy]-4,8-di-tert-butyl-2,10-dimethoxy-5,7-dioxa-6-phosphadibenzo[a,c]cycloheptene

There total 1 articles about 6-[(diphenylphosphanyl)methoxy]-4,8-di-tert-butyl-2,10-dimethoxy-5,7-dioxa-6-phosphadibenzo[a,c]cycloheptene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 240134-26-3,108609-95-6
4,8-di-tert-butyl-6-chloro-2,10-dimethoxy-5,7,6-dioxaphosphadibenzo[a,c]cycloheptene

: 5958-44-1
diphenylphosphinomethanol

: 425429-85-2
6-[(diphenylphosphanyl)methoxy]-4,8-di-tert-butyl-2,10-dimethoxy-5,7-dioxa-6-phosphadibenzo[a,c]cycloheptene

Guidance literature:: With triethylamine; In toluene; at 20 ℃;
DOI:10.1016/S0957-4166(00)00227-5

Reference yield: 90.0%

: 12266-72-7
(1,5-cylooctadiene)di-iodoplatinum(II)

: 425429-85-2
6-[(diphenylphosphanyl)methoxy]-4,8-di-tert-butyl-2,10-dimethoxy-5,7-dioxa-6-phosphadibenzo[a,c]cycloheptene

: 425429-98-7
[Pt((C₆H₅)2PCH₂OP(OC₆H₂C(CH₃)3OCH₃)2)I₂]

Guidance literature:: In toluene; addn. of the solid ligand, (N2); filtration, washing (toluene, hexane), vac. drying, elem. anal.;
DOI:10.1002/1099-0682(200203)2002:3<711::AID-EJIC711>3.0.CO;2-E

Reference yield: 88.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 425429-85-2
6-[(diphenylphosphanyl)methoxy]-4,8-di-tert-butyl-2,10-dimethoxy-5,7-dioxa-6-phosphadibenzo[a,c]cycloheptene

: 425429-96-5
[Pd((C₆H₅)2PCH₂OP(OC₆H₂C(CH₃)3OCH₃)2)Cl₂]

Guidance literature:: In toluene; dropwise addn. of the phosphine ligand in soln. (N2), 30 min; vac. concn., addn. of hexane, washing (hexane), vac. drying; elem. anal.;
DOI:10.1002/1099-0682(200203)2002:3<711::AID-EJIC711>3.0.CO;2-E