tert-butyl (3R,4R,5R)-3,4,6-tris(benzyloxy)-5-(methylsulfonyloxy)-2-methylenehexylcarbamate

Base Information

Chemical Name:tert-butyl (3R,4R,5R)-3,4,6-tris(benzyloxy)-5-(methylsulfonyloxy)-2-methylenehexylcarbamate
CAS No.:1161011-50-2
Molecular Formula:C₃₄H₄₃NO₈S
Molecular Weight:625.783
Hs Code.:

Synonyms:tert-butyl (3R,4R,5R)-3,4,6-tris(benzyloxy)-5-(methylsulfonyloxy)-2-methylenehexylcarbamate

Suppliers and Price of tert-butyl (3R,4R,5R)-3,4,6-tris(benzyloxy)-5-(methylsulfonyloxy)-2-methylenehexylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl (3R,4R,5R)-3,4,6-tris(benzyloxy)-5-(methylsulfonyloxy)-2-methylenehexylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl (3R,4R,5R)-3,4,6-tris(benzyloxy)-5-(methylsulfonyloxy)-2-methylenehexylcarbamate

There total 1 articles about tert-butyl (3R,4R,5R)-3,4,6-tris(benzyloxy)-5-(methylsulfonyloxy)-2-methylenehexylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.5%

: 1161011-49-9
tert-butyl (3R,4S,5R)-3,4,6-tris(benzyloxy)-5-hydroxy-2-methylenehexylcarbamate

: 124-63-0
methanesulfonyl chloride

: 1161011-50-2
tert-butyl (3R,4R,5R)-3,4,6-tris(benzyloxy)-5-(methylsulfonyloxy)-2-methylenehexylcarbamate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1002/ejoc.200801301

Reference yield: 70.5%

: 1161011-50-2
tert-butyl (3R,4R,5R)-3,4,6-tris(benzyloxy)-5-(methylsulfonyloxy)-2-methylenehexylcarbamate

: 1161011-51-3
(2S,3S,4R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-methylenepiperidine

Guidance literature:: tert-butyl (3R,4R,5R)-3,4,6-tris(benzyloxy)-5-(methylsulfonyloxy)-2-methylenehexylcarbamate; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 0.833333h;

With potassium carbonate; In acetonitrile; at 20 - 70 ℃; for 8h;
DOI:10.1002/ejoc.200801301