6-(4-Chloro-phenyl)-1-methyl-3-methylsulfanyl-1H-[1,2,4]triazolo[4,3-b][1,2,4]triazole

Base Information

Chemical Name:6-(4-Chloro-phenyl)-1-methyl-3-methylsulfanyl-1H-[1,2,4]triazolo[4,3-b][1,2,4]triazole
CAS No.:86663-35-6
Molecular Formula:C₁₁H₁₀ClN₅S
Molecular Weight:279.753
Hs Code.:

Synonyms:6-(4-Chloro-phenyl)-1-methyl-3-methylsulfanyl-1H-[1,2,4]triazolo[4,3-b][1,2,4]triazole

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Chemical Property of 6-(4-Chloro-phenyl)-1-methyl-3-methylsulfanyl-1H-[1,2,4]triazolo[4,3-b][1,2,4]triazole

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Technology Process of 6-(4-Chloro-phenyl)-1-methyl-3-methylsulfanyl-1H-[1,2,4]triazolo[4,3-b][1,2,4]triazole

There total 4 articles about 6-(4-Chloro-phenyl)-1-methyl-3-methylsulfanyl-1H-[1,2,4]triazolo[4,3-b][1,2,4]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 86663-42-5
4-(4'-Chlorobenzamidino)-1-methyl-3,5-bis-1,2,4-triazolium iodide

: 86663-35-6
6-(4-Chloro-phenyl)-1-methyl-3-methylsulfanyl-1H-[1,2,4]triazolo[4,3-b][1,2,4]triazole

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; for 24h; Heating;
DOI:10.1055/s-1983-30363

Reference yield:

: 623-03-0
4-Cyanochlorobenzene

: 86663-35-6
6-(4-Chloro-phenyl)-1-methyl-3-methylsulfanyl-1H-[1,2,4]triazolo[4,3-b][1,2,4]triazole

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / KOC₄H₉-t / 2-methyl-propan-2-ol / 3 h / Heating

2: 72 percent / methanol / 7 h / Heating

3: 100 percent / KOC₄H₉-t / 2-methyl-propan-2-ol / 24 h / Heating

With potassium tert-butylate; In methanol; tert-butyl alcohol;
DOI:10.1055/s-1983-30363

Reference yield:

: 86663-45-8
N-(3,5-Bis-methylsulfanyl-[1,2,4]triazol-4-yl)-4-chloro-benzamidine

: 86663-35-6
6-(4-Chloro-phenyl)-1-methyl-3-methylsulfanyl-1H-[1,2,4]triazolo[4,3-b][1,2,4]triazole

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / methanol / 7 h / Heating

2: 100 percent / KOC₄H₉-t / 2-methyl-propan-2-ol / 24 h / Heating

With potassium tert-butylate; In methanol; tert-butyl alcohol;
DOI:10.1055/s-1983-30363