N,N-dimethylformamide di-tert-pentoxyacetal

Base Information

• Chemical Name: N,N-dimethylformamide di-tert-pentoxyacetal
• CAS No.: 1174130-81-4
• Molecular Formula: C₁₃H₂₉NO₂
• Molecular Weight: 231.379

Synonyms:N,N-dimethylformamide di-tert-pentoxyacetal

Chemical Property of N,N-dimethylformamide di-tert-pentoxyacetal

Chemical Property:

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Technology Process of N,N-dimethylformamide di-tert-pentoxyacetal

There total 1 articles about N,N-dimethylformamide di-tert-pentoxyacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N,N',N'-Tetramethylformamidinium chloride (1071-38-1) + sodium tert-pentoxide (14593-46-5) → tris(dimethylamino)methane (5762-56-1) + tert-pentoxy-bis(dimethylamino)methane (147196-94-9) + N,N-dimethylformamide di-tert-pentoxyacetal (1174130-81-4)

Guidance literature:

In tetrahydrofuran; toluene; at 20 ℃; for 48h; Product distribution / selectivity;

Reference yield:

(S)-2-biphenyl-4-ylmethyl-5-oxopyrrolidine-1-carboxylic acid tert-butyl ester (1038924-77-4) + tris(dimethylamino)methane (5762-56-1) + tert-pentoxy-bis(dimethylamino)methane (147196-94-9) + N,N-dimethylformamide di-tert-pentoxyacetal (1174130-81-4) → (R)-5-biphenyl-4-ylmethyl-3-[1-dimethylaminometh-(E/Z)-ylidene]-2-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester (1174130-65-4)

Guidance literature:

at 80 ℃; for 2h; Product distribution / selectivity;

upstream raw materials:

N,N,N',N'-Tetramethylformamidinium chloride

sodium tert-pentoxide

Downstream raw materials:

(R)-5-biphenyl-4-ylmethyl-3-[1-dimethylaminometh-(E/Z)-ylidene]-2-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester

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