6-amino-5-[(cyclohexylamino)methyl]-3-methyl-2-(methylthio)pyrimidin-4(3H)-one

Base Information

• Chemical Name: 6-amino-5-[(cyclohexylamino)methyl]-3-methyl-2-(methylthio)pyrimidin-4(3H)-one
• CAS No.: 1638842-54-2
• Molecular Formula: C₁₃H₂₂N₄OS
• Molecular Weight: 282.41

Synonyms:6-amino-5-[(cyclohexylamino)methyl]-3-methyl-2-(methylthio)pyrimidin-4(3H)-one

Chemical Property of 6-amino-5-[(cyclohexylamino)methyl]-3-methyl-2-(methylthio)pyrimidin-4(3H)-one

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Technology Process of 6-amino-5-[(cyclohexylamino)methyl]-3-methyl-2-(methylthio)pyrimidin-4(3H)-one

There total 1 articles about 6-amino-5-[(cyclohexylamino)methyl]-3-methyl-2-(methylthio)pyrimidin-4(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C7H9N3O2S (1228343-85-8) + cyclohexylamine (108-91-8,157973-60-9) → 6-amino-5-[(cyclohexylamino)methyl]-3-methyl-2-(methylthio)pyrimidin-4(3H)-one (1638842-54-2)

Guidance literature:

With sodium tris(acetoxy)borohydride; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.3998/ark.5550190.p008.653

Reference yield: 69.0%

6-amino-5-[(cyclohexylamino)methyl]-3-methyl-2-(methylthio)pyrimidin-4(3H)-one (1638842-54-2) + orthoformic acid triethyl ester (122-51-0) → 6-cyclohexyl-3-methyl-2-(methylthio)-5,6-dihydropyrimido[4,5-d]pyrimidin-4(3H)-one (1638842-46-2)

Guidance literature:

With acetic acid; In neat (no solvent); at 150 ℃; for 0.0166667h; Sealed tube; Microwave irradiation;

DOI:10.3998/ark.5550190.p008.653

Reference yield: 67.0%

6-amino-5-[(cyclohexylamino)methyl]-3-methyl-2-(methylthio)pyrimidin-4(3H)-one (1638842-54-2) + benzaldehyde (100-52-7) → 6-cyclohexyl-3-methyl-2-(methylthio)-7-phenyl-5,6,7,8-tetrahydropyrimido[4,5-d]pyrimidin-4(3H)-one (1638842-34-8)

Guidance literature:

With 10-camphorsufonic acid; In ethanol; at 50 ℃; for 22h;

DOI:10.3998/ark.5550190.p008.653

upstream raw materials:

C₇H₉N₃O₂S

cyclohexylamine

Downstream raw materials:

6-cyclohexyl-3-methyl-2-(methylthio)-5,6-dihydropyrimido[4,5-d]pyrimidin-4(3H)-one

6-cyclohexyl-3,7-dimethyl-2-(methylthio)-5,6-dihydropyrimido[4,5-d]pyrimidin-4(3H)-one

6-cyclohexyl-3-methyl-2-(methylthio)-7-phenyl-5,6,7,8-tetrahydropyrimido[4,5-d]pyrimidin-4(3H)-one

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