1,2-di-O-palmitoyl-3-O-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

Base Information

Chemical Name:1,2-di-O-palmitoyl-3-O-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol
CAS No.:1192755-07-9
Molecular Formula:C₇₈H₁₂₇NO₁₀
Molecular Weight:1238.87
Hs Code.:

Synonyms:1,2-di-O-palmitoyl-3-O-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

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Chemical Property of 1,2-di-O-palmitoyl-3-O-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

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Technology Process of 1,2-di-O-palmitoyl-3-O-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

There total 19 articles about 1,2-di-O-palmitoyl-3-O-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1192755-06-8
1,2-dipalmitoyl-3-O-(6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucosyl)-sn-glycerol

: 57-10-3
1-hexadecylcarboxylic acid

: 1192755-07-9
1,2-di-O-palmitoyl-3-O-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; In dichloromethane; at 20 ℃; for 21h; Inert atmosphere;
DOI:10.1016/j.carres.2009.05.022

Reference yield: 76.0%

: 1383450-05-2
3-O-(6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

: 112-67-4
n-hexadecanoyl chloride

: 1192755-07-9
1,2-di-O-palmitoyl-3-O-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

Guidance literature:: With dmap; In pyridine; at 20 ℃; for 4h;
DOI:10.1016/j.carres.2012.04.005

Reference yield:

: 1192755-03-5
3-O-(6'-azido-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-1,2-O-isopropylidene-sn-glycerol

: 1192755-07-9
1,2-di-O-palmitoyl-3-O-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

2: triphenylphosphine / tetrahydrofuran; water / 5 h / 50 °C

3: dmap / pyridine / 4 h / 20 °C

With dmap; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; pyridine; methanol; water;
DOI:10.1016/j.carres.2012.04.005