C₅₆H₆₈N₆Si₂

Base Information

Chemical Name:C₅₆H₆₈N₆Si₂
CAS No.:265670-98-2
Molecular Formula:C₅₆H₆₈N₆Si₂
Molecular Weight:881.367
Hs Code.:

C<sub>56</sub>H<sub>68</sub>N<sub>6</sub>Si<sub>2</sub>

Synonyms:C₅₆H₆₈N₆Si₂

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Chemical Property of C₅₆H₆₈N₆Si₂

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Technology Process of C₅₆H₆₈N₆Si₂

There total 11 articles about C₅₆H₆₈N₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 769-92-6
4-tert-Butylaniline

: 265670-98-2
C₅₆H₆₈N₆Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: BnNEt₃⁽¹⁺⁾*ICl₂^(1-); CaCO₃ / CH₂Cl₂; methanol

2.1: sodium nitrite; HCl / acetonitrile; H₂O

2.2: potassium carbonate / H₂O

2.3: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

3.1: iodomethane / 120 °C

4.1: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

5.1: potassium carbonate / methanol; tetrahydrofuran

6.1: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

7.1: tetra-n-butylammonium fluoride / tetrahydrofuran; ethanol

8.1: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; calcium carbonate; benzyl triethylammonium dichloroiodate; sodium nitrite; methyl iodide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetonitrile; 1.1: Iodination / 2.1: Diazotization / 2.2: Substitution / 2.3: Substitution / 3.1: Decomposition / 4.1: Substitution / 5.1: Hydrolysis / 6.1: Substitution / 7.1: Hydrolysis / 8.1: Substitution;
DOI:10.1021/ol005623w

Reference yield:

: C₂₄H₃₉N₃Si₂

: 265670-98-2
C₅₆H₆₈N₆Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: iodomethane / 120 °C

2: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

3: potassium carbonate / methanol; tetrahydrofuran

4: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

5: tetra-n-butylammonium fluoride / tetrahydrofuran; ethanol

6: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; methyl iodide; In tetrahydrofuran; methanol; ethanol; 1: Decomposition / 2: Substitution / 3: Hydrolysis / 4: Substitution / 5: Hydrolysis / 6: Substitution;
DOI:10.1021/ol005623w

Reference yield:

: 615-43-0
2-iodophenylamine

: 265670-98-2
C₅₆H₆₈N₆Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: conc. HCl; NaNO₂ / H₂O; acetonitrile / 0.5 h / -5 - 0 °C

1.2: potassium carbonate / H₂O; acetonitrile / 0.25 h

2.1: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

3.1: tetra-n-butylammonium fluoride / tetrahydrofuran; ethanol

4.1: copper(I) iodide; triethylamine; PdCl₂(PPh₃)2

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; sodium nitrite; In tetrahydrofuran; ethanol; water; acetonitrile; 1.1: Diazotization / 1.2: Substitution / 2.1: Substitution / 3.1: Hydrolysis / 4.1: Substitution;
DOI:10.1021/ol005623w