3-(p-anisyl)-1,2,4-triazolo<3,4-c>pyrimido<4,5-b>tetrahydrobenzothiophene

Base Information

Chemical Name:3-(p-anisyl)-1,2,4-triazolo<3,4-c>pyrimido<4,5-b>tetrahydrobenzothiophene
CAS No.:81154-34-9
Molecular Formula:C₁₈H₁₆N₄OS
Molecular Weight:336.417
Hs Code.:

Synonyms:3-(p-anisyl)-1,2,4-triazolo<3,4-c>pyrimido<4,5-b>tetrahydrobenzothiophene

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Chemical Property of 3-(p-anisyl)-1,2,4-triazolo<3,4-c>pyrimido<4,5-b>tetrahydrobenzothiophene

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Technology Process of 3-(p-anisyl)-1,2,4-triazolo<3,4-c>pyrimido<4,5-b>tetrahydrobenzothiophene

There total 3 articles about 3-(p-anisyl)-1,2,4-triazolo<3,4-c>pyrimido<4,5-b>tetrahydrobenzothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 81154-30-5
4-methoxy-benzaldehyde (5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4-yl)hydrazone

: 81154-34-9
3-(p-anisyl)-1,2,4-triazolo<3,4-c>pyrimido<4,5-b>tetrahydrobenzothiophene

Guidance literature:: With bromine; sodium acetate; In acetic acid; for 0.5h; Ambient temperature;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 81154-34-9
3-(p-anisyl)-1,2,4-triazolo<3,4-c>pyrimido<4,5-b>tetrahydrobenzothiophene

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / ethanol / 1 h / Heating

2: 67 percent / sodium acetate, bromine / acetic acid / 0.5 h / Ambient temperature

With bromine; sodium acetate; In ethanol; acetic acid;

Reference yield:

: 40106-45-4
4-hydrazino-5,6-tetramethylenothieno<2,3-d>pyrimidine

: 81154-34-9
3-(p-anisyl)-1,2,4-triazolo<3,4-c>pyrimido<4,5-b>tetrahydrobenzothiophene

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / ethanol / 1 h / Heating

2: 67 percent / sodium acetate, bromine / acetic acid / 0.5 h / Ambient temperature

With bromine; sodium acetate; In ethanol; acetic acid;